Benzenemethanol, a-(2-chloroethyl)-, acetate

Base Information

• Chemical Name: Benzenemethanol, a-(2-chloroethyl)-, acetate
• CAS No.: 22912-90-9
• Molecular Formula: C11H13ClO2
• Molecular Weight: 212.676

Synonyms:

Chemical Property of Benzenemethanol, a-(2-chloroethyl)-, acetate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanol, a-(2-chloroethyl)-, acetate

There total 4 articles about Benzenemethanol, a-(2-chloroethyl)-, acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.5%

vinyl acetate (108-05-4,9003-20-7) + 3-chloro-1-phenyl-propan-1-ol (18776-12-0,125712-82-5) → (RS)-3-chloro-1-phenyl-1-propyl acetate (22912-90-9)

Guidance literature:

With lipase A from candida antarctica; In hexane; at 20 ℃; for 24h; Enzymatic reaction;

DOI:10.1055/s-0030-1260149

Reference yield: 74.0%

3-chloro-1-phenyl-propan-1-ol (18776-12-0,125712-82-5) + acetic anhydride (108-24-7) → (RS)-3-chloro-1-phenyl-1-propyl acetate (22912-90-9)

Guidance literature:

With tantalum pentachloride; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4039(98)00465-1

Reference yield:

acetyl chloride (75-36-5) → (RS)-3-chloro-1-phenyl-1-propyl acetate (22912-90-9)

Guidance literature:

With pyridine; diethyl ether;

DOI:10.1021/ja01561a046

upstream raw materials:

3-chloro-1-phenyl-propan-1-ol

acetic anhydride

acetyl chloride

vinyl acetate

Downstream raw materials:

3-chloro-1-phenylpropanol

(1R)-3-chloro-1-phenylpropanol

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