Butanamide, 2-amino-N,N,3-trimethyl- (9CI)

Base Information

• Chemical Name: Butanamide, 2-amino-N,N,3-trimethyl- (9CI)
• CAS No.: 230643-41-1
• Molecular Formula: C7H16N2O
• Molecular Weight: 144.21500
• Hs Code.: 2924199090
• Mol file: 230643-41-1.mol

Synonyms:rac-trichostatic acid;rac-valine N,N-dimethylamide;2-amino-3-methyl butanoic acid dimethylamide;trichostatic acid;

Chemical Property of Butanamide, 2-amino-N,N,3-trimethyl- (9CI)

Chemical Property:

• PSA: 46.33000
• LogP: 0.75820

Purity/Quality:

99% ^*data from raw suppliers

2-Amino-N,N,3-trimethyl-butanamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Butanamide, 2-amino-N,N,3-trimethyl- (9CI)

There total 1 articles about Butanamide, 2-amino-N,N,3-trimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D,L-valine (516-06-3,25609-85-2,7004-03-7,921-10-8) + dimethyl amine (124-40-3) → 2-amino-3-methyl butanoic acid dimethylamide (230643-41-1)

Guidance literature:

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1039/b211914e

Reference yield: 94.0%

2-amino-3-methyl butanoic acid dimethylamide (230643-41-1) + Nα-phthaloyl-L-phenylalanine (5123-55-7) → 2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3-phenyl-propionylamino]-3,N,N-trimethyl-butyramide

Guidance literature:

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1039/b211914e

Reference yield: 44.0%

(S)-N-(benzyloxycarbonyl)valine (1149-26-4) + 2-amino-3-methyl butanoic acid dimethylamide (230643-41-1) → [(S)-1-((R)-1-Dimethylcarbamoyl-2-methyl-propylcarbamoyl)-2-methyl-propyl]-carbamic acid benzyl ester

Guidance literature:

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1039/b211914e

upstream raw materials:

D,L-valine

dimethyl amine

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