5(4H)-Isoxazolone, 4-methyl-3-phenyl-

Base Information

Chemical Name:5(4H)-Isoxazolone, 4-methyl-3-phenyl-
CAS No.:23244-37-3
Molecular Formula:C10H9NO2
Molecular Weight:175.187
Hs Code.:
Mol file:23244-37-3.mol

Synonyms:4-methyl-3-phenyl-2H-isoxazol-5-one;4-methyl-3-phenylisoxazoline-5-one;4-Methyl-3-phenylisoxazolin-5-one;3-Phenyl-4-methyl-isoxazolin-5-on;4-methyl-3-phenylisoxazol-5-one;

Suppliers and Price of 5(4H)-Isoxazolone, 4-methyl-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5(4H)-Isoxazolone, 4-methyl-3-phenyl-

Chemical Property:

PSA：38.66000
LogP:1.01920

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5(4H)-Isoxazolone, 4-methyl-3-phenyl-

There total 6 articles about 5(4H)-Isoxazolone, 4-methyl-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10488-87-6
ethyl 2-benzoylpropionate

: 23244-37-3
4-methyl-3-phenylisoxazole-5(4H)-one

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; at 60 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201410933

Reference yield:

: 32742-19-1,116782-25-3,29540-54-3
methyl 2-benzoylpropionate

: 23244-37-3
4-methyl-3-phenylisoxazole-5(4H)-one

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; at 78 ℃;
DOI:10.1002/adsc.202001200

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 23244-37-3
4-methyl-3-phenylisoxazole-5(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil / 20 h / 22 °C / Inert atmosphere

2: hydroxylamine hydrochloride; pyridine / ethanol / 16 h / 60 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; sodium hydride; In ethanol; mineral oil;
DOI:10.1002/anie.201410933