Butanoic acid, 4-(dimethylamino)-, [4-chloro-2-[[2-oxo-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-3(2H)-yl ]methyl]phenoxy]methyl ester

Base Information

Chemical Name:Butanoic acid, 4-(dimethylamino)-, [4-chloro-2-[[2-oxo-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-3(2H)-yl ]methyl]phenoxy]methyl ester
CAS No.:234433-20-6
Molecular Formula:C₂₃H₂₃ClF₃N₃O₅
Molecular Weight:513.901
Hs Code.:

Butanoic acid, 4-(dimethylamino)-,
[4-chloro-2-[[2-oxo-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-3(2H)-yl
]methyl]phenoxy]methyl ester

Synonyms:

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Chemical Property of Butanoic acid, 4-(dimethylamino)-, [4-chloro-2-[[2-oxo-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-3(2H)-yl ]methyl]phenoxy]methyl ester

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Technology Process of Butanoic acid, 4-(dimethylamino)-, [4-chloro-2-[[2-oxo-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-3(2H)-yl ]methyl]phenoxy]methyl ester

There total 4 articles about Butanoic acid, 4-(dimethylamino)-, [4-chloro-2-[[2-oxo-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-3(2H)-yl ]methyl]phenoxy]methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69954-66-1
4-(dimethylamino)butyric acid hydrochloride

: 233676-45-4
3-[(5-Chloro-2-[(chloromethyl)oxy]phenyl)methyl]-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-2(3 H)-one

: 234433-20-6
[4-chloro-2-[[5-[4-(trifluoromethyl)phenyl]-2,3-dihydro-2-oxo-1,3,4-oxadiazol-3-yl]methyl]phenoxy]methyl-4-(dimethylamino)butyrate

Guidance literature:: With caesium carbonate; In acetone; at 23 ℃;
DOI:10.1016/S0960-894X(03)00296-8

Reference yield:

: 202821-81-6
3-[(5-Chloro-2-hydroxyphenyl)methyl]-5-[4-(trifluoromethyl)-phenyl]-1,3,4-oxadiazol-2(3H)-one

: 234433-20-6
[4-chloro-2-[[5-[4-(trifluoromethyl)phenyl]-2,3-dihydro-2-oxo-1,3,4-oxadiazol-3-yl]methyl]phenoxy]methyl-4-(dimethylamino)butyrate

Guidance literature:: Multi-step reaction with 3 steps

1: NaH; HMPA

2: SO₂Cl₂ / CH₂Cl₂

3: Cs₂CO₃ / acetone / 23 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; sulfuryl dichloride; sodium hydride; caesium carbonate; In dichloromethane; acetone;
DOI:10.1016/S0960-894X(03)00296-8

Reference yield:

: 233676-37-4
3-[(5-chloro-2-[(methylthiomethyl)oxy]-phenyl)methyl]-5-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-2(3H)-one

: 234433-20-6
[4-chloro-2-[[5-[4-(trifluoromethyl)phenyl]-2,3-dihydro-2-oxo-1,3,4-oxadiazol-3-yl]methyl]phenoxy]methyl-4-(dimethylamino)butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / CH₂Cl₂

2: Cs₂CO₃ / acetone / 23 °C

With sulfuryl dichloride; caesium carbonate; In dichloromethane; acetone;
DOI:10.1016/S0960-894X(03)00296-8