4,4'-BIS(HEPTYLOXY)AZOXYBENZENE

Base Information

• Chemical Name: 4,4'-BIS(HEPTYLOXY)AZOXYBENZENE
• CAS No.: 2635-26-9
• Molecular Formula: C₂₆H₃₈N₂O₃
• Molecular Weight: 426.599
• Mol file: 2635-26-9.mol

Synonyms:Azoxybenzene,4,4'-bis(heptyloxy)- (6CI,7CI,8CI); Diazene, bis[4-(heptyloxy)phenyl]-, 1-oxide(9CI); 4,4'-Bis(heptyloxy)azoxybenzene; 4,4'-Diheptoxyazoxybenzene;4,4'-Diheptyloxyazoxybenzene; NSC 171005; p,p'-Diheptyloxyazoxybenzene;p-Diheptyloxyazoxybenzene

Chemical Property of 4,4'-BIS(HEPTYLOXY)AZOXYBENZENE

Chemical Property:

• Melting Point: 73-122 °C
• Refractive Index: 1.5300 (estimate)
• Boiling Point: 553.3°Cat760mmHg
• Flash Point: 288.4°C
• PSA: 59.57000
• Density: 1.02g/cm³
• LogP: 8.83390
• Storage Temp.: Flammables area

Purity/Quality:

99% ^*data from raw suppliers

4,4'-Diheptyloxyazoxybenzene ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn-F
• Statements: 36/37/38-20/22-11
• Safety Statements: 37/39-26-16

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4'-BIS(HEPTYLOXY)AZOXYBENZENE

There total 7 articles about 4,4'-BIS(HEPTYLOXY)AZOXYBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-(heptyloxy)-4-nitrobenzene (13565-36-1) → bis-(4-heptyloxy-phenyl)-diazene N-oxide (2635-26-9,70906-50-2)

Guidance literature:

With bismuth; at 20 ℃; for 3h;

DOI:10.1021/jo0203645

Reference yield:

→ bis-(4-heptyloxy-phenyl)-diazene N-oxide (2635-26-9,70906-50-2)

Guidance literature:

DOI:10.1021/ja01077a039

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → bis-(4-heptyloxy-phenyl)-diazene N-oxide (2635-26-9,70906-50-2)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: 87 percent / bismuth / 3 h / 20 °C

With bismuth; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jo0203645

upstream raw materials:

1-(heptyloxy)-4-nitrobenzene

4-nitro-phenol

1-Bromoheptane

potassium 4-nitrophenolate

Refernces