6-chloro-5-nitronicotinoyl chloride

Base Information Edit

Chemical Name:6-chloro-5-nitronicotinoyl chloride
CAS No.:23945-84-8
Molecular Formula:C6H2Cl2N2O3
Molecular Weight:220.99800
Hs Code.:
Mol file:23945-84-8.mol

Synonyms:6-chloro-5-nitronicotinoyl chloride;

Suppliers and Price of 6-chloro-5-nitronicotinoyl chloride

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 6-chloro-5-nitronicotinoyl chloride Edit

Chemical Property:

PSA：75.78000
LogP:2.54540

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-chloro-5-nitronicotinoyl chloride

There total 6 articles about 6-chloro-5-nitronicotinoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7477-10-3
6-chloro-5-nitronicotinic acid

: 23945-84-8
6-chloro-5-nitro-nicotinoyl chloride

Guidance literature:: With thionyl chloride; for 5h; Reflux;

Reference yield:

: 6635-31-0
6-hydroxy-5-nitronicotinic acid

: 23945-84-8
6-chloro-5-nitro-nicotinoyl chloride

Guidance literature:: With trichlorophosphate; Heating / reflux;

Reference yield:

: 1603-41-4
(5-methyl-pyridin-2-yl)amine

: 23945-84-8
6-chloro-5-nitro-nicotinoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid; sulfuric acid / 2 h / 0 - 5 °C

1.2: 4 h / Cooling with ice

2.1: trichlorophosphate / 5 h / Reflux

3.1: sodium dichromate; sulfuric acid / 12 h / 25 °C / Cooling with ice

4.1: thionyl chloride / 5 h / Reflux

With thionyl chloride; sodium dichromate; sulfuric acid; nitric acid; trichlorophosphate;