2,2'-BIPYRIDINE-6(1H)-THIONE

Base Information

Chemical Name:2,2'-BIPYRIDINE-6(1H)-THIONE
CAS No.:239798-76-6
Molecular Formula:C10H8N2S
Molecular Weight:188.24900
Hs Code.:
Mol file:239798-76-6.mol

Synonyms:6-(pyridin-2-yl)pyridine-2(1H)-thione;6-mercapto-2,2'-bipyridine;2,2'-BIPYRIDINE-6(1H)-THIONE;2,2'-BINAPHTHALENE-6,6'-DICARBOXYLIC ACID;

Suppliers and Price of 2,2'-BIPYRIDINE-6(1H)-THIONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,2'-BIPYRIDINE-6(1H)-THIONE 95.00%
5MG
$ 499.40

Total 1 raw suppliers

Chemical Property of 2,2'-BIPYRIDINE-6(1H)-THIONE

Chemical Property:

Boiling Point:354.7oC at 760 mmHg
Flash Point:168.3oC
PSA：64.58000
Density:1.29g/cm3
LogP:2.43230

Purity/Quality:: 2,2'-BIPYRIDINE-6(1H)-THIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2'-BIPYRIDINE-6(1H)-THIONE

There total 4 articles about 2,2'-BIPYRIDINE-6(1H)-THIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 13040-77-2
6-Chloro-[2,2']bipyridinyl

: 239798-76-6
6-mercapto-2,2'-bipyridine

Guidance literature:: With sodium hydrogen sulfide monohydrate; In N,N-dimethyl-formamide;
DOI:10.1039/b810569c

Reference yield: 78.0%

: 10495-73-5
2-bromo-6-(pyridin-2-yl)pyridine

: 239798-76-6
6-mercapto-2,2'-bipyridine

Guidance literature:: With potassium hydroxide; sodium hydrogensulfide; In N,N-dimethyl-formamide; Heating;
DOI:10.1039/b606715h

Reference yield:

: 366-18-7
[2,2]bipyridinyl

: 239798-76-6
6-mercapto-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / m-chloroperbenzoic acid / CHCl₃ / 13 h / Ambient temperature

2: 41 percent / POCl₃ / 12 h / Heating

3: 80 percent / KSH / dimethylformamide / 4 h / Heating

With potassium hydrosulfide; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00885-0