Gold, (4-fluorophenyl)(triphenylphosphine)-

Base Information

Chemical Name:Gold, (4-fluorophenyl)(triphenylphosphine)-
CAS No.:24228-71-5
Molecular Formula:C24H19AuFP
Molecular Weight:554.354
Hs Code.:
Mol file:24228-71-5.mol

Synonyms:

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Chemical Property of Gold, (4-fluorophenyl)(triphenylphosphine)-

Chemical Property:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Gold, (4-fluorophenyl)(triphenylphosphine)-

There total 3 articles about Gold, (4-fluorophenyl)(triphenylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 1765-93-1
4-fluoroboronic acid

: 24228-71-5
(4-fluorophenyl)(triphenylphosphine)gold(I)

Guidance literature:: With caesium carbonate; In isopropyl alcohol; at 50 ℃; for 22h;
DOI:10.1021/jacs.7b06668

Reference yield: 85.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 352-13-6
4-flourophenylmagnesium bromide

: 24228-71-5
(4-fluorophenyl)(triphenylphosphine)gold(I)

Guidance literature:: In tetrahydrofuran; 4-fluorophenylmagnesium bromide added dropwise at -78°C to soln. ClAuPPh3 in THF in Schlenk techniques under Ar; mixt. warmed to room temp., mixed for 16 h; treated with satd. soln. of NH4Cl, extd. with Et2O; org. layers washed with satd. soln. of NaCl, dried over MgSO4; solvents removed under vac.; crystals obtained via crystn. from CHCl3;
DOI:10.1016/j.jorganchem.2005.07.080

Reference yield: 67.0%

: 53317-87-6
tris[triphenylphosphinegold(I)]oxonium tetrafluoroborate

: 352-13-6
4-flourophenylmagnesium bromide

: 24228-71-5
(4-fluorophenyl)(triphenylphosphine)gold(I)

Guidance literature:: In tetrahydrofuran; diethyl ether; addn. of ethereal Mg-compd. to a stirred suspension of Au-compd. in THF, stirred for 3 h at 30°C; treated with H2O, organic layer sepd., washed (H2O), dried (K2CO3), passed through column (alumina), evapd. (vac.), diluted with petroleum ether;
DOI:10.1007/BF01157354