Butanoic acid, 2-hydroxy-3-methyl-, phenylmethyl ester

Base Information Edit

Chemical Name:Butanoic acid, 2-hydroxy-3-methyl-, phenylmethyl ester
CAS No.:2441-07-8
Molecular Formula:C12H16O3
Molecular Weight:208.257
Hs Code.:
Mol file:2441-07-8.mol

Synonyms:

Suppliers and Price of Butanoic acid, 2-hydroxy-3-methyl-, phenylmethyl ester

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Butanoic acid, 2-hydroxy-3-methyl-, phenylmethyl ester Edit

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanoic acid, 2-hydroxy-3-methyl-, phenylmethyl ester

There total 13 articles about Butanoic acid, 2-hydroxy-3-methyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 17407-56-6
(R)-2-Hydroxy-3-methylbutyric acid

: 100-51-6,185532-71-2
benzyl alcohol

: 2441-07-8,65138-05-8,14487-24-2
benzyl (R)-2-hydroxy-3-methylbutanoate

Guidance literature:: benzyl alcohol; With toluene-4-sulfonic acid; In benzene; for 0.5h; Reflux;

(R)-2-Hydroxy-3-methylbutyric acid; In benzene; Reflux;
DOI:10.1016/j.bmcl.2011.10.094

Reference yield: 87.0%

: 76585-78-9
phenylmethyl 3-methyl-2-oxobutanoate

: 2441-07-8
(+/-)-2-hydroxy-3-methylbutyric acid benzyl ester

Guidance literature:: phenylmethyl 3-methyl-2-oxobutanoate; With sodium tris(acetoxy)borohydride; In ethanol; at 20 ℃; for 22.0833h;

With sodium hydrogencarbonate; In ethanol; water; pH=9;

Reference yield: 80.0%

: 17407-56-6
(R)-2-Hydroxy-3-methylbutyric acid

: 100-39-0
benzyl bromide

: 2441-07-8,65138-05-8,14487-24-2
benzyl (R)-2-hydroxy-3-methylbutanoate

Guidance literature:: (R)-2-Hydroxy-3-methylbutyric acid; With caesium carbonate; In N,N-dimethyl-formamide; at 0 ℃; for 0.666667h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 15h; Inert atmosphere;
DOI:10.1002/chem.201504457