2-Cyano-3,3-bis(methylsulfanyl)prop-2-enethioamide

Base Information

Chemical Name:2-Cyano-3,3-bis(methylsulfanyl)prop-2-enethioamide
CAS No.:24571-57-1
Molecular Formula:C6H8N2S3
Molecular Weight:204.341
Hs Code.:
NSC Number:687618
DSSTox Substance ID:DTXSID40388258
Nikkaji Number:J900.246D
Mol file:24571-57-1.mol

Synonyms:NSC687618;2-cyano-3,3-bis(methylsulfanyl)prop-2-enethioamide;24571-57-1;2-Propenethioamide, 2-cyano-3,3-bis(methylthio)-;DTXSID40388258;NSC-687618;2-Cyano-3,3-bis(methylthio)acrylthiamide

Suppliers and Price of 2-Cyano-3,3-bis(methylsulfanyl)prop-2-enethioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Cyano-3,3-bis(methylsulfanyl)prop-2-enethioamide

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:203.98496178
Heavy Atom Count:11
Complexity:230

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSC(=C(C#N)C(=S)N)SC

Technology Process of 2-Cyano-3,3-bis(methylsulfanyl)prop-2-enethioamide

There total 1 articles about 2-Cyano-3,3-bis(methylsulfanyl)prop-2-enethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 7357-70-2
Cyanothioacetamide

: 74-88-4
methyl iodide

: 24571-57-1
2-Cyano-3,3-bis-methylsulfanyl-thioacrylamide

Guidance literature:: With sodium ethanolate; Yield given. Multistep reaction; 1.) reflux, 20 min; reflux, 20 min, 2.) EtOH;

Reference yield: 85.0%

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 24571-57-1
2-Cyano-3,3-bis-methylsulfanyl-thioacrylamide

: 2-cyano-3-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylamino)-3-methylsulfanyl-thioacrylamide

Guidance literature:: With piperidine; In ethanol; for 0.5h; Heating;
DOI:10.1081/SCC-120014787

Reference yield:

: 24571-57-1
2-Cyano-3,3-bis-methylsulfanyl-thioacrylamide

: 7-imino-1,7a-dimethyl-5-methylsulfanyl-3-oxo-2-phenyl-2,3,7,7a-tetrahydro-1H-pyrazolo[4,3-b]pyridine-6-carbothioic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / piperidine / ethanol / 0.5 h / Heating

2: 60 percent / conc. HCl / ethanol / 0.5 h / Heating

With piperidine; hydrogenchloride; In ethanol;
DOI:10.1081/SCC-120014787