Diazene, [(hydroxyimino)phenylmethyl](4-methylphenyl)-

Base Information

Chemical Name:Diazene, [(hydroxyimino)phenylmethyl](4-methylphenyl)-
CAS No.:24621-46-3
Molecular Formula:C₁₄H₁₃N₃O
Molecular Weight:239.277
Hs Code.:

Synonyms:

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Chemical Property of Diazene, [(hydroxyimino)phenylmethyl](4-methylphenyl)-

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Technology Process of Diazene, [(hydroxyimino)phenylmethyl](4-methylphenyl)-

There total 1 articles about Diazene, [(hydroxyimino)phenylmethyl](4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1858-99-7
benzaldehyde p-tolylhydrazone

: 110-46-3
isopentyl nitrite

: 24621-46-3
p-tolylazo-benzaldoxime

Guidance literature:: With ethanol; sodium ethanolate;
DOI:10.1039/jr9410000823

Reference yield: 70.0%

: cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

: sodium perchlorate

: 24621-46-3
p-tolylazo-benzaldoxime

: {Ru((C₅H₄N)2)2(N(OH)CC₆H₅NNC₆H₄CH₃)}⁽²⁺⁾*2(ClO₄)^(1-)*H₂O={Ru((C₅H₄N)2)2(N(OH)CC₆H₅NNC₆H₄CH₃)}(ClO₄)2*H₂O

Guidance literature:: With HClO₄; In methanol; water; org. compd. added to Ru complex in MeOH-H2O, mixture refluxed for 2 h, filtered, aq. NaClO4 contg. HClO4 added to filtrate; filtration, washing (H2O, C6H6, Et2O), drying in vac.; elem. anal.;
DOI:10.1039/DT9830000961

Reference yield: 59.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 24621-46-3
p-tolylazo-benzaldoxime

: 7550-35-8
lithium bromide

: 78149-19-6
trans-dibromo[α-(p-tolylazo)benzaldoximato-N,N''][α-(p-tolylazo)benzaldoxime-N,N'']ruthenium(III)

Guidance literature:: In methanol; ligand was added to soln. of Ru salt after stirring with LiBr for 10 min; cooling, filtration, washing with water and aq. EtOH; drying in vac. over P4O10; dissoln. in CH2Cl2; chromy. on silica gel (benzene); evapn.; elem. anal.;
DOI:10.1021/ic50224a003