3(2H)-Pyridazinone,2-(methoxymethyl)-6-phenyl-5-[(trimethylsilyl)ethynyl]-

Base Information

Chemical Name:3(2H)-Pyridazinone,2-(methoxymethyl)-6-phenyl-5-[(trimethylsilyl)ethynyl]-
CAS No.:247158-85-6
Molecular Formula:C17H20N2O2Si
Molecular Weight:312.444
Hs Code.:

Synonyms:3(2H)-Pyridazinone,2-(methoxymethyl)-6-phenyl-5-[(trimethylsilyl)ethynyl]-

Suppliers and Price of 3(2H)-Pyridazinone,2-(methoxymethyl)-6-phenyl-5-[(trimethylsilyl)ethynyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3(2H)-Pyridazinone,2-(methoxymethyl)-6-phenyl-5-[(trimethylsilyl)ethynyl]-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 3(2H)-Pyridazinone,2-(methoxymethyl)-6-phenyl-5-[(trimethylsilyl)ethynyl]-

There total 2 articles about 3(2H)-Pyridazinone,2-(methoxymethyl)-6-phenyl-5-[(trimethylsilyl)ethynyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 247158-79-8
5-Bromo-2-methoxymethyl-6-phenylpyridazin-3-one

: 1066-54-2
trimethylsilylacetylene

: 247158-85-6
2-methoxymethyl-6-phenyl-5-(2-trimethylsilanylethynyl)-3-pyridazinone

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 55 ℃; for 3h;
DOI:10.1016/S0040-4020(03)00263-1

Reference yield:

: 90766-97-5
5-bromo-6-phenylpyridazin-3(2H)-one

: 247158-85-6
2-methoxymethyl-6-phenyl-5-(2-trimethylsilanylethynyl)-3-pyridazinone

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / CH₂Cl₂

2: 90 percent / PdCl₂(PPh₃)2; CuI; Et₃N / dimethylformamide / 3 h / 55 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 2: Sonogashira reaction;
DOI:10.1016/S0040-4020(03)00263-1