4'-(4-Hydroxyphenylazo)acetophenone

Base Information

• Chemical Name: 4'-(4-Hydroxyphenylazo)acetophenone
• CAS No.: 2496-16-4
• Molecular Formula: C14H12N2O2
• Molecular Weight: 240.261
• European Community (EC) Number: 661-508-1
• DSSTox Substance ID: DTXSID90422277
• Nikkaji Number: J1.677.916D
• Mol file: 2496-16-4.mol

Synonyms:4'-(4-HYDROXYPHENYLAZO)ACETOPHENONE;2496-16-4;4-[(4-acetylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one;4-hydroxy-4'-acetylazobenzene;DTXSID90422277;MFCD00161177;AKOS001584202;AKOS024340784;SR-01000087525;SR-01000087525-1

Chemical Property of 4'-(4-Hydroxyphenylazo)acetophenone

Chemical Property:

• XLogP3: 3.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 240.089877630
• Heavy Atom Count: 18
• Complexity: 301

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)C1=CC=C(C=C1)N=NC2=CC=C(C=C2)O

Technology Process of 4'-(4-Hydroxyphenylazo)acetophenone

There total 5 articles about 4'-(4-Hydroxyphenylazo)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

p-aminobenzophenone (99-92-3) + phenol (108-95-2,27073-41-2) → C14H12N2O2 (2496-16-4)

Guidance literature:

p-aminobenzophenone; With hydrogenchloride; sodium nitrite; In water; at 2 ℃;

phenol; With sodium hydroxide;

DOI:10.1016/j.molliq.2014.12.022

Reference yield:

C13H18N3O (132402-15-4) + phenol (108-95-2,27073-41-2) → 1-[4-(4-hydroxy-phenylazo)-phenyl]-ethanone (2496-16-4)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; Yield given; 1.) 0 deg C, 5 min, 2.) 0 deg C, 20 min;

DOI:10.1007/BF01169720

Reference yield:

→ 1-[4-(4-hydroxy-phenylazo)-phenyl]-ethanone (2496-16-4)

Guidance literature:

With sulfuric acid;

upstream raw materials:

4-Acetyl-phenyl-diazonium

phenol

C₁₃H₁₈N₃O

p-aminobenzophenone

Downstream raw materials:

1-[4-(4-acetoxy-phenylazo)-phenyl]-ethanone