Benzoic acid, 3-[(1-methyl-4-piperidinyl)oxy]-

Base Information

• Chemical Name: Benzoic acid, 3-[(1-methyl-4-piperidinyl)oxy]-
• CAS No.: 250681-61-9
• Molecular Formula: C13H17NO3
• Molecular Weight: 235.27900
• Mol file: 250681-61-9.mol

Synonyms:3-(1-Methyl-piperidin-4-yloxy)-benzoic acid;3-(1-methylpiperidin-4-yloxy)benzoic acid;

Chemical Property of Benzoic acid, 3-[(1-methyl-4-piperidinyl)oxy]-

Chemical Property:

• Boiling Point: 386.6±32.0 °C(Predicted)
• PSA: 49.77000
• Density: 1.179±0.06 g/cm3(Predicted)
• LogP: 1.79570

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 3-[(1-methyl-4-piperidinyl)oxy]-

There total 1 articles about Benzoic acid, 3-[(1-methyl-4-piperidinyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-(N-methyl-4'-piperidinyloxy)benzoic acid (250681-61-9)

Guidance literature:

Reference yield:

3-(N-methyl-4'-piperidinyloxy)benzoic acid (250681-61-9) + oxalyl dichloride (79-37-8) + N-(3-amino-4-chlorophenyl)-4-cyanobenzamide (250681-58-4) → N-[2-chloro-5-(4-cyanobenzamido)phenyl]-3-(1-methylpiperidin-4-yloxy)benzamide (250680-52-5)

Guidance literature:

With pyridine; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

3-(N-methyl-4'-piperidinyloxy)benzoic acid (250681-61-9) + (S)-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid (4-pentylphenyl)amide (862506-74-9) → (S)-2-[3-(1-Methyl-piperidin-4-yloxy)-benzoyl]-1,2,3,4-tetrahydro-isoquinoline-3-carboxylic acid (4-pentyl-phenyl)-amide

Guidance literature:

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In chloroform;

DOI:10.1016/j.bmcl.2005.02.041

Downstream raw materials:

N-[2-chloro-5-(4-cyanobenzamido)phenyl]-3-(1-methylpiperidin-4-yloxy)benzamide

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