Benzene, [(3-cyclopenten-1-ylmethoxy)methyl]-

Base Information

Chemical Name:Benzene, [(3-cyclopenten-1-ylmethoxy)methyl]-
CAS No.:260443-67-2
Molecular Formula:C13H16O
Molecular Weight:188.269
Hs Code.:
DSSTox Substance ID:DTXSID60460464

Synonyms:260443-67-2;Benzene, [(3-cyclopenten-1-ylmethoxy)methyl]-;SCHEMBL880157;DTXSID60460464

Suppliers and Price of Benzene, [(3-cyclopenten-1-ylmethoxy)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, [(3-cyclopenten-1-ylmethoxy)methyl]-

Chemical Property:

PSA：9.23000
LogP:3.16940
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:188.120115130
Heavy Atom Count:14
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C=CCC1COCC2=CC=CC=C2

Technology Process of Benzene, [(3-cyclopenten-1-ylmethoxy)methyl]-

There total 2 articles about Benzene, [(3-cyclopenten-1-ylmethoxy)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 25125-21-7
4-(hydroxymethyl)cyclopentene

: 100-39-0
benzyl bromide

: 260443-67-2
4-[(phenylmethoxy)methyl]-3-cyclopentene

Guidance literature:: 4-(hydroxymethyl)cyclopentene; With sodium hydride; In tetrahydrofuran; at 23 ℃; for 0.5h;

benzyl bromide; With tert-Butyl iodide; In tetrahydrofuran; at 23 ℃; for 8h;
DOI:10.1016/S0040-4020(02)01531-4

Reference yield:

: 7686-77-3
3-cyclopentene-1-carboxylic acid

: 260443-67-2
4-[(phenylmethoxy)methyl]-3-cyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 23 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 23 °C

2.2: 97 percent / tert-butyl iodide / tetrahydrofuran / 8 h / 23 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(02)01531-4