Benzene, 1,1'-[(2-methylene-1,3-propanediyl)bis(oxymethylene)]bis-

Base Information

Chemical Name:Benzene, 1,1'-[(2-methylene-1,3-propanediyl)bis(oxymethylene)]bis-
CAS No.:27441-79-8
Molecular Formula:C18H20O2
Molecular Weight:268.356
Hs Code.:
DSSTox Substance ID:DTXSID60440084
Nikkaji Number:J2.092.552C
Wikidata:Q82256273

Synonyms:Benzene, 1,1'-[(2-methylene-1,3-propanediyl)bis(oxymethylene)]bis-;27441-79-8;DTXSID60440084;1,3-Bis(benzyloxy)-2-methylenepropane

Suppliers and Price of Benzene, 1,1'-[(2-methylene-1,3-propanediyl)bis(oxymethylene)]bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzene, 1,1'-[(2-methylene-1,3-propanediyl)bis(oxymethylene)]bis-

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:8
Exact Mass:268.146329876
Heavy Atom Count:20
Complexity:237

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(COCC1=CC=CC=C1)COCC2=CC=CC=C2

Technology Process of Benzene, 1,1'-[(2-methylene-1,3-propanediyl)bis(oxymethylene)]bis-

There total 4 articles about Benzene, 1,1'-[(2-methylene-1,3-propanediyl)bis(oxymethylene)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3513-81-3
2-(Hydroxymethyl)allyl alcohol

: 100-39-0
benzyl bromide

: 27441-79-8
2-methylenepropane-1,3-bisbenzyl ether

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 40 ℃;
DOI:10.1039/b401100g

Reference yield: 98.0%

: 1871-57-4
2-chloromethyl-3-chloroprop-1-ene

: 100-51-6,185532-71-2
benzyl alcohol

: 27441-79-8
2-methylenepropane-1,3-bisbenzyl ether

Guidance literature:: 2-chloromethyl-3-chloroprop-1-ene; benzyl alcohol; With sodium hydride; In tetrahydrofuran; for 0.5h; Cooling with ice;

With 15-crown-5; In tetrahydrofuran; for 14h; Reflux;
DOI:10.1021/ol301263v

Reference yield: 20.0%

: 3513-81-3
2-(Hydroxymethyl)allyl alcohol

: 100-39-0
benzyl bromide

: 27441-79-8
2-methylenepropane-1,3-bisbenzyl ether

: 109240-66-6
2?(benzyloxymethyl)prop?2?en?1?ol

Guidance literature:: 2-(Hydroxymethyl)allyl alcohol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

With water; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.09.106