Benzene, 1-nitro-4-(trimethoxymethyl)-

Base Information

Chemical Name:Benzene, 1-nitro-4-(trimethoxymethyl)-
CAS No.:27689-97-0
Molecular Formula:C10H13NO5
Molecular Weight:227.217
Hs Code.:
DSSTox Substance ID:DTXSID901283573

Synonyms:Benzene, 1-nitro-4-(trimethoxymethyl)-;DTXSID901283573;AKOS011076193;27689-97-0

Suppliers and Price of Benzene, 1-nitro-4-(trimethoxymethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-nitro-4-(trimethoxymethyl)-

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:227.07937252
Heavy Atom Count:16
Complexity:220

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(C1=CC=C(C=C1)[N+](=O)[O-])(OC)OC

Technology Process of Benzene, 1-nitro-4-(trimethoxymethyl)-

There total 4 articles about Benzene, 1-nitro-4-(trimethoxymethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 27689-97-0
trimethyl 4-nitroorthobenzoate

Guidance literature:: With boron trifluoride; In Hexadecane; at 110 ℃; for 6h; Autoclave;

Reference yield:

: 67-56-1
methanol

: [Dimethoxy-(4-nitro-phenyl)-methyl]-methyl-phenyl-amine

: 27689-97-0
trimethyl 4-nitroorthobenzoate

: 100-61-8
N-methylaniline

Guidance literature:: With acetic acid; for 0.166667h; Yield given;
DOI:10.1021/jo00318a032

Reference yield:

: 961-61-5
N-methyl-N-phenyl-4-nitrobenzamide

: 27689-97-0
trimethyl 4-nitroorthobenzoate

Guidance literature:: Multi-step reaction with 3 steps

2: 1.) sodium / 1.) - 2.) CH₂Cl₂, 30 min

3: glacial acetic acid / 0.17 h

With sodium; acetic acid;
DOI:10.1021/jo00318a032