Trigermane, 1,1,1,3,3,3-hexaphenyl-2-(triphenylgermyl)-

Base Information

Chemical Name:Trigermane, 1,1,1,3,3,3-hexaphenyl-2-(triphenylgermyl)-
CAS No.:2816-38-8
Molecular Formula:C54H46Ge4
Molecular Weight:985.319
Hs Code.:

Synonyms:

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Chemical Property of Trigermane, 1,1,1,3,3,3-hexaphenyl-2-(triphenylgermyl)-

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Technology Process of Trigermane, 1,1,1,3,3,3-hexaphenyl-2-(triphenylgermyl)-

There total 3 articles about Trigermane, 1,1,1,3,3,3-hexaphenyl-2-(triphenylgermyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 7782-65-2
germane

: 1265901-88-9
(Ph₃Ge)3GeNMe₂

: 2816-38-8
(Ph₃Ge)3GeH

Guidance literature:: In acetonitrile; byproducts: Me2NH; (N2); Schlenk technique; GeH4 was condensed into soln. of Ge compd. in MeCN at 77 K; warmed to room temp.; heated at 85°C for 18 h; evapd. (vac.); elem. anal.;
DOI:10.1021/om101091c

Reference yield: 64.0%

: 16853-85-3
lithium aluminium tetrahydride

: 139599-12-5
triphenylgermanetriflate

: 2816-38-8
(Ph₃Ge)3GeH

Guidance literature:: In diethyl ether; byproducts: LiO3SCF3; (N2); std. Schlenk technique; soln. of Ge compd. in Et2O was treated with soln. of LiAlH4 in Et2O; stirred at room temp. for 4 h; volatiles removed (vac.); dissolved in C6H6; filtered through Celite; pad washed (C6H6); solvent removed (vac.); elem. anal.;
DOI:10.1021/om800040f

Reference yield:

: 112168-56-6
PhGe(GePh₃)3

: 2816-38-8
(Ph₃Ge)3GeH

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform-d1

2: diethyl ether

In diethyl ether; chloroform-d1;
DOI:10.1021/om800040f