Acetic acid, chloro[(3,4-dichlorophenyl)hydrazono]-, ethyl ester

Base Information

Chemical Name:Acetic acid, chloro[(3,4-dichlorophenyl)hydrazono]-, ethyl ester
CAS No.:28317-50-2
Molecular Formula:C10H9Cl3N2O2
Molecular Weight:295.55000
Hs Code.:
Mol file:28317-50-2.mol

Synonyms:ethyl chloro[2-(3,4-dichlorophenyl)hydrazinylidene]ethanoate;2-Chlor-2-(3,4-dichlorphenylhydrazono)-essigsaeureethylester;chloro[(3,4-dichlorophenyl)hydrazono]-acetic acid,ethyl ester;Acetic acid,chloro[(3,4-dichlorophenyl)hydrazono]-,ethyl ester;

Suppliers and Price of Acetic acid, chloro[(3,4-dichlorophenyl)hydrazono]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Acetic acid, chloro[(3,4-dichlorophenyl)hydrazono]-, ethyl ester

Chemical Property:

PSA：50.69000
LogP:3.59370

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetic acid, chloro[(3,4-dichlorophenyl)hydrazono]-, ethyl ester

There total 3 articles about Acetic acid, chloro[(3,4-dichlorophenyl)hydrazono]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 95-76-1
m,p-dichloroaniline

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 28317-50-2
ethyl chloro[2-(3,4-dichlorophenyl)hydrazinylidene]ethanoate

Guidance literature:: m,p-dichloroaniline; With hydrogenchloride; sodium nitrite; In water; at 0 ℃;

ethyl 2-chloro-3-oxo-butyrate; With sodium acetate; In ethanol; water; at 0 ℃; for 4h;
DOI:10.1055/s-0030-1260026

Reference yield:

: 105-39-5
chloroacetic acid ethyl ester

: 95-76-1
m,p-dichloroaniline

: 28317-50-2
<(3,4-dichlorophenyl)hydrazino>chloromethylenecarboxylate

Guidance literature:: With hydrogenchloride; sodium acetate; sodium nitrite; Yield given. Multistep reaction; 1.) EtOH, 2.) EtOH, 4 h;
DOI:10.1021/jm00378a006