4-(3-Methyl-1-oxo-2-butenyl)morpholine

Base Information

Chemical Name:4-(3-Methyl-1-oxo-2-butenyl)morpholine
CAS No.:53868-72-7
Molecular Formula:C₉H₁₅NO₂
Molecular Weight:169.224
Hs Code.:2934999090
Mol file:53868-72-7.mol

Synonyms:Morpholine,4-(3-methyl-1-oxo-2-butenyl);3-methyl-1-(morpholin-4-yl)but-2-en-1-one;4-[1-oxo-3-methyl-2-butenyl]morpholine;3-Methyl-2-butenoic acid,morpholide;4-[(2E)-1-oxo-3-methyl-2-butenyl]morpholine;N-ssss-Me2-acryloylmorpholin;4-(3-methyl-crotonoyl)-morpholine;4-(3-Methyl-1-oxo-2-butenyl)morpholine;4-(3-methyl-but-2-enoyl)-morpholine;4-(3-Methyl-crotonoyl)-morpholin;

Suppliers and Price of 4-(3-Methyl-1-oxo-2-butenyl)morpholine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-(3-METHYL-1-OXO-2-BUTENYL)MORPHOLINE 95.00%
5MG
$ 498.45

Total 3 raw suppliers

Chemical Property of 4-(3-Methyl-1-oxo-2-butenyl)morpholine

Chemical Property:

Vapor Pressure:0.000274mmHg at 25°C
Boiling Point:322.7°Cat760mmHg
Flash Point:149°C
PSA：29.54000
Density:1.039g/cm³
LogP:0.74930

Purity/Quality:

99% ^*data from raw suppliers

4-(3-METHYL-1-OXO-2-BUTENYL)MORPHOLINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(3-Methyl-1-oxo-2-butenyl)morpholine

There total 4 articles about 4-(3-Methyl-1-oxo-2-butenyl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 110-91-8,99108-56-2
morpholine

: 541-47-9
3-Methylbutenoic acid

: 53868-72-7
4-[(2E)-1-oxo-3-methyl-2-butenyl]morpholine

Guidance literature:: With N-ethylmorpholine;; N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; In dichloromethane; at 20 - 25 ℃; for 2h;
DOI:10.1055/s-1984-30857

Reference yield: 45.0%

: 15159-40-7
4-morpholinocarbonyl chloride

: 38614-36-7
2-methylpropen-1-ylmagnesium bromide

: 53868-72-7
4-[(2E)-1-oxo-3-methyl-2-butenyl]morpholine

Guidance literature:: 2-methylpropen-1-ylmagnesium bromide; With CuCN; In diethyl ether; at -30 ℃; for 0.75h;

4-morpholinocarbonyl chloride; In diethyl ether; at -30 - 20 ℃; for 15h;
DOI:10.1021/ol0487130