Benzo[b]thiophene, 5-chloro-3-phenyl-

Base Information

Chemical Name:Benzo[b]thiophene, 5-chloro-3-phenyl-
CAS No.:28540-36-5
Molecular Formula:C14H9ClS
Molecular Weight:244.744
Hs Code.:
DSSTox Substance ID:DTXSID00479474
Nikkaji Number:J1.316.460F
Mol file:28540-36-5.mol

Synonyms:Benzo[b]thiophene, 5-chloro-3-phenyl-;28540-36-5;5-Chloro-3-phenyl-benzo[b]thiophene;SCHEMBL11617762;DTXSID00479474

Suppliers and Price of Benzo[b]thiophene, 5-chloro-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Benzo[b]thiophene, 5-chloro-3-phenyl-

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:244.0113492
Heavy Atom Count:16
Complexity:237

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CSC3=C2C=C(C=C3)Cl

Technology Process of Benzo[b]thiophene, 5-chloro-3-phenyl-

There total 7 articles about Benzo[b]thiophene, 5-chloro-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 849403-96-9
trifluoro-methanesulfonic acid 5-chloro-benzo[b]thiophen-3-yl ester

: 98-80-6
phenylboronic acid

: 28540-36-5
5-chloro-3-phenylbenzo[b]thiophene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾;
DOI:10.1055/s-2004-837230

Reference yield: 66.0%

: 20532-33-6
5-chlorobenzothiophene

: 109674-45-5
4-methyl-2,6-dioxo-8-phenylhexahydro-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-4-ium-8-uide

: 28540-36-5
5-chloro-3-phenylbenzo[b]thiophene

Guidance literature:: With trifluorormethanesulfonic acid; C₂₄H₃₆N₂O₂Pd*2C₂H₄O₂; cesium trifluoroacetate; trifluoroacetic acid; p-benzoquinone; silver(l) oxide; In water; at 50 ℃; for 20h; Temperature; regioselective reaction;
DOI:10.1055/s-0034-1379606

Reference yield:

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 536-74-3
phenylacetylene

: 28540-36-5
5-chloro-3-phenylbenzo[b]thiophene

: 7205-65-4
tert-butyl (4-chlorophenyl) sulfide

: 57488-23-0
E-3-[(4-chlorophenyl)sulfanyl]-2-phenyl-2-propenenitrile

: 92103-31-6
1-chloro-4-(2-phenylvinylsulfanyl)benzene

Guidance literature:: With meta-dinitrobenzene; In benzene; at 20 ℃; for 24h; Further byproducts given. Title compound not separated from byproducts; Irradiation;
DOI:10.1021/jo991871y