2-bromophenazine 10-oxide

Base Information

Chemical Name:2-bromophenazine 10-oxide
CAS No.:3224-57-5
Molecular Formula:C12H7BrN2O
Molecular Weight:275.1008
Hs Code.:
Mol file:3224-57-5.mol

Synonyms:

Suppliers and Price of 2-bromophenazine 10-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2-bromophenazine 10-oxide

Chemical Property:

Vapor Pressure:5E-08mmHg at 25°C
Boiling Point:454.8°Cat760mmHg
Flash Point:228.8°C
Density:1.66g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-bromophenazine 10-oxide

There total 5 articles about 2-bromophenazine 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 273-09-6
benzofurazan

: 139139-81-4
bis(4-bromophenyl)iodonium triflate

: 3224-57-5
3-bromophenazine 5-oxide

Guidance literature:: With copper(I) bromide; In 1,2-dichloro-ethane; at 70 ℃; for 24h; regioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01748

Reference yield:

: 88-74-4
2-nitro-aniline

: 3224-57-5
3-bromophenazine 5-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; sodium hypochlorite / ethanol; water / 0 °C / Sealed tube; Inert atmosphere

2: triethyl phosphite / tetrahydrofuran / 7 h / 60 °C / Inert atmosphere; Sealed tube

3: copper(I) bromide / 1,2-dichloro-ethane / 24 h / 70 °C / Sealed tube; Inert atmosphere

With sodium hypochlorite; potassium hydroxide; copper(I) bromide; triethyl phosphite; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane;
DOI:10.1021/acs.orglett.8b01748

Reference yield:

: 480-96-6,68100-26-5
benzofurazan oxide

: 3224-57-5
3-bromophenazine 5-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: triethyl phosphite / tetrahydrofuran / 7 h / 60 °C / Inert atmosphere; Sealed tube

2: copper(I) bromide / 1,2-dichloro-ethane / 24 h / 70 °C / Sealed tube; Inert atmosphere

With copper(I) bromide; triethyl phosphite; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/acs.orglett.8b01748