(Z)-2,7-Dimethyl-3-octen-5-yne

Base Information

• Chemical Name: (Z)-2,7-Dimethyl-3-octen-5-yne
• CAS No.: 28935-76-4
• Molecular Formula: C10H16
• Molecular Weight: 136.23400
• Mol file: 28935-76-4.mol

Synonyms:cis-2,7-dimethyl oct-5-yn-3-ene;2,7-Dimethyl-cis-3-okten-5-in;2,7-dimethyl-oct-3c-en-5-yne;2,7-Dimethyl-cis-3-octen-5-in;3-Octen-5-yne,2,7-dimethyl;

Chemical Property of (Z)-2,7-Dimethyl-3-octen-5-yne

Chemical Property:

• PSA: 0.00000
• LogP: 2.85800

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (Z)-2,7-Dimethyl-3-octen-5-yne

There total 6 articles about (Z)-2,7-Dimethyl-3-octen-5-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

3-methyl-but-1-yne (598-23-2) + isopropylamine (75-31-0) → 2,7-Dimethyl-cis-3-octen-5-in (28935-76-4) + Isopropyl-[3-methyl-but-(Z)-ylidene]-amine (41807-54-9) + N-isopropyl-(3-methyl-2-butylidene)amine (160285-17-6) + 2,4-diisopropyl-1-butene-3-yne

Guidance literature:

With [(Et₂N)3U][BPh₄]; In benzene; at 80 ℃; for 6h;

DOI:10.1002/1521-3765(20021202)8:23<5384::AID-CHEM5384>3.0.CO;2-X

Reference yield: 47.0%

3-methyl-but-1-yne (598-23-2) + ethylamine (75-04-7,85404-22-4) → [1,2-Dimethyl-prop-(Z)-ylidene]-ethyl-amine (55007-51-7) + 2,7-Dimethyl-cis-3-octen-5-in (28935-76-4) + 2,4-diisopropyl-1-butene-3-yne + Ethyl-[3-methyl-but-(Z)-ylidene]-amine

Guidance literature:

With [(Et₂N)3U][BPh₄]; In benzene; at 20 ℃; for 40h;

DOI:10.1002/1521-3765(20021202)8:23<5384::AID-CHEM5384>3.0.CO;2-X

Reference yield: 40.0%

3-methyl-but-1-yne (598-23-2) + tert-butylamine (75-64-9) → 2,7-Dimethyl-cis-3-octen-5-in (28935-76-4) + N-tert-butyl-iso-pentalimine (56175-48-5) + 2,4-diisopropyl-1-butene-3-yne + (Z)-2,9-Dimethyl-5,6-bis-[2-methyl-prop-(Z)-ylidene]-dec-3-en-7-yne

Guidance literature:

With [(Et₂N)3U][BPh₄]; In benzene; at 80 ℃; for 37h;

DOI:10.1002/1521-3765(20021202)8:23<5384::AID-CHEM5384>3.0.CO;2-X

upstream raw materials:

1,4-diisopropyl-1,3-butadiyne

3-methyl-but-1-yne

tert-Butyl-dideuteroamin

ethylamine

Downstream raw materials:

2,7-dimethyl-3(Z),5(Z)-octadiene

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