Diethyl (4-butoxyphenyl)propanedioate

Base Information

Chemical Name:Diethyl (4-butoxyphenyl)propanedioate
CAS No.:29148-20-7
Molecular Formula:C17H24O5
Molecular Weight:308.375
Hs Code.:
DSSTox Substance ID:DTXSID80496381
Wikidata:Q82345190
Mol file:29148-20-7.mol

Synonyms:Diethyl (4-butoxyphenyl)propanedioate;29148-20-7;DTXSID80496381

Suppliers and Price of Diethyl (4-butoxyphenyl)propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl (4-butoxyphenyl)propanedioate

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:11
Exact Mass:308.16237386
Heavy Atom Count:22
Complexity:316

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCOC1=CC=C(C=C1)C(C(=O)OCC)C(=O)OCC

Technology Process of Diethyl (4-butoxyphenyl)propanedioate

There total 7 articles about Diethyl (4-butoxyphenyl)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 96693-04-8
1-(n-butoxy)-4-iodobenzene

: 105-53-3
diethyl malonate

: 29148-20-7
diethyl (4-butoxyphenyl)malonate

Guidance literature:: With copper(l) iodide; caesium carbonate; 2-Phenylphenol; for 17h; Heating;
DOI:10.1039/b608012j

Reference yield:

: 105-56-6
ethyl 2-cyanoacetate

: 29148-20-7
diethyl (4-butoxyphenyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium t-butoxide / 2.) dichlorobis(triphenylphosphine)palladium / 1.) 1,2-dimethoxyethane, room temperature, 10 min, 2.) 1,2-dimethoxyethane, 70 deg C, 8 h

2: concd. hydrochloric acid, calcium chloride / benzene / 1.) room temperature, 3 h, 2.) 55 deg C, 2 h, 3.) reflux, 5 h

With hydrogenchloride; potassium tert-butylate; calcium chloride; bis-triphenylphosphine-palladium(II) chloride; In benzene;
DOI:10.1246/bcsj.62.3896

Reference yield:

: 64-17-5
ethanol

: 103126-09-6
ethyl 4-butoxyphenylcyanoacetate

: 29148-20-7
diethyl (4-butoxyphenyl)malonate

Guidance literature:: With hydrogenchloride; calcium chloride; In benzene; 1.) room temperature, 3 h, 2.) 55 deg C, 2 h, 3.) reflux, 5 h;
DOI:10.1246/bcsj.62.3896