4-Methacrylamido-2,2,6,6-tetramethylpiperidine

Base Information

• Chemical Name: 4-Methacrylamido-2,2,6,6-tetramethylpiperidine
• CAS No.: 31582-46-4
• Molecular Formula: C13H24N2O
• Molecular Weight: 224.34
• European Community (EC) Number: 889-493-9
• DSSTox Substance ID: DTXSID30592024
• Nikkaji Number: J3.500.732F
• Wikidata: Q82485916
• Mol file: 31582-46-4.mol

Synonyms:31582-46-4;4-METHACRYLAMIDO-2,2,6,6-TETRAMETHYLPIPERIDINE;n-(2,2,6,6-tetramethylpiperidin-4-yl)methacrylamide;2-Methyl-N-(2,2,6,6-tetramethylpiperidin-4-yl)prop-2-enamide;MATP;SCHEMBL109129;DTXSID30592024;2-Methyl-N-(2,2,6,6-tetramethyl-4-piperidinyl)-2-propenamide;MFCD16293856;DB-263151;F72250;J-018481

Chemical Property of 4-Methacrylamido-2,2,6,6-tetramethylpiperidine

Chemical Property:

• Boiling Point: 351.6±42.0 °C(Predicted)
• PKA: 14.65±0.60(Predicted)
• Density: 0.96±0.1 g/cm3(Predicted)
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 224.188863393
• Heavy Atom Count: 16
• Complexity: 289

Purity/Quality:

97% ^*data from raw suppliers

4-Methacrylamido-2,2,6,6-tetramethylpiperidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)C(=O)NC1CC(NC(C1)(C)C)(C)C
• Uses: A 4-aminopiperidine derivative for stabilizing synthetic polymers against photo and thermal decomposition.

Technology Process of 4-Methacrylamido-2,2,6,6-tetramethylpiperidine

There total 3 articles about 4-Methacrylamido-2,2,6,6-tetramethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE (36768-62-4) + poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) → N-(2,2,6,6-tetramethylpiperidin-4-yl)methacrylamide (31582-46-4)

Guidance literature:

With chloroformic acid ethyl ester;

DOI:10.1021/acs.biomac.5b00599

Reference yield: 78.0%

4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE (36768-62-4) + Methacryloyl chloride (920-46-7,26937-45-1) → N-(2,2,6,6-tetramethylpiperidin-4-yl)methacrylamide (31582-46-4)

Guidance literature:

With triethylamine; In chloroform; at 0 ℃; for 6h;

DOI:10.1021/acs.macromol.5b01367

Reference yield:

→ N-(2,2,6,6-tetramethylpiperidin-4-yl)methacrylamide (31582-46-4)

Guidance literature:

entspr. 4-Aminoverb., Methacryloylchlorid, Et3N;

upstream raw materials:

4-AMINO-2,2,6,6-TETRAMETHYLPIPERIDINE

Methacryloyl chloride

poly(methacrylic acid)

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