COPPER(I) ACETATE

Base Information

• Chemical Name: COPPER(I) ACETATE
• CAS No.: 598-54-9
• Molecular Formula: C₂H₃O₂*Cu
• Molecular Weight: 122.591
• Hs Code.: 29152900
• Mol file: 598-54-9.mol

Synonyms:Aceticacid, copper(1+) salt (8CI,9CI);Copper acetate (CuOAc) (6CI);Coppermonoacetate;Copper(1+) acetate;Copper(I) acetate;Cuprous acetate;

Chemical Property of COPPER(I) ACETATE

Chemical Property:

• Appearance/Colour: Pale green or khaki powder
• Melting Point: 250 °C (dec.)(lit.)
• Boiling Point: decomposes if strongly heated [MER06]
• PSA: 26.30000
• LogP: 0.01130
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature
• Sensitive.: moisture sensitive
• Water Solubility.: rapidly hydrolyzed by H2O to form yellow Cu2O [MER06]

Purity/Quality:

99%, ^*data from raw suppliers

Copper(I) acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Copper acetate(CuOAc) was used as a starting material for the preparation of copper nanoparticles and CuAlO2 p-type nanostructured semiconductors.

Technology Process of COPPER(I) ACETATE

There total 28 articles about COPPER(I) ACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

→ tert-butyl peroxyacetate (107-71-1) + copper (I) acetate (598-54-9,142-71-2,4180-12-5,24381-58-6,66760-61-0,66760-62-1)

Guidance literature:

Reference yield: 65.0%

stannous octoate + copper diacetate (142-71-2) → Sn(4+)*2CH3(CH2)3CH(C2H5)COO(1-)*2CH3COO(1-)=Sn(CH3(CH2)3CH(C2H5)COO)2(CH3COO)2 + copper (I) acetate (598-54-9,142-71-2,4180-12-5,24381-58-6,66760-61-0,66760-62-1)

Guidance literature:

In dichloromethane; mixt. of copper(II) acetate and tin(II) 2-ethylhexanoate in CH2Cl2 is stirred at room temp. for 4 h; filtration, product is washed with CH2Cl2, solid dried in vacuo for several hours; elem. anal.;

DOI:10.1016/S0277-5387(00)84170-4

Reference yield: 63.0%

acetic acid (64-19-7,77671-22-8) + copper(l) chloride → copper (I) acetate (598-54-9,142-71-2,4180-12-5,24381-58-6,66760-61-0,66760-62-1)

Guidance literature:

With triethylamine; In dichloromethane; (N2); CH3COOH added to a suspn. of CuCl at 25°C, stirred for 10 min, a soln. of (C2H5)3N added, stirred at 25°C for 5 h; filtered off, washed (CH2Cl2), dried (vac.);

DOI:10.1002/zaac.200800189

upstream raw materials:

copper diacetate

acetic acid

ammonium acetate

copper(II) acetate monohydrate

Downstream raw materials:

(3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one

acetic anhydride

4,5-difluoro-2-[[1-(2-pyridinyl)-1H-pyrazol-5-yl]amino]benzoic acid

4-chloro-3-ethyl-6,7-difluoro-1-(2-pyridinyl)-1H-pyrazolo[3,4-b]quinoline

Refernces

Copper chalcogenide clusters stabilized with ferrocene-based diphosphine ligands

10.1021/ic3021854

The study focuses on the synthesis and characterization of copper(I) chalcogenide clusters stabilized by the redox-active diphosphine ligand 1,1′-bis(diphenylphosphino)ferrocene (dppf). The researchers used copper(I) acetate coordination complex (dppf)CuOAc (5) and reacted it with 0.5 equivalents of E(SiMe3)2 (where E = S, Se, Te) to prepare the clusters [Cu12(μ4-S)6(μ-dppf)4] (1), [Cu8(μ4-Se)4(μ-dppf)3] (2), [Cu4(μ4-Te)(μ4-η2-Te2)(μ-dppf)2] (3), and [Cu12(μ5-Te)4(μ8-η2-Te2)2(μ-dppf)4] (4). These chalcogenide clusters serve to explore the utility of the bidentate phosphine-based ferrocene ligand for the surface passivation of copper chalcogen frameworks, with the dppf ligands playing a crucial role in stabilizing the {Cu2xEx} cores and protecting the clusters from decomposition or further condensation into bulk solids. The study aimed to understand the redox properties and coordination abilities of these clusters, which could have implications for the development of functional materials.

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