4-Chloro-2,3-dihydro-1H-inden-1-OL

Base Information

Chemical Name:4-Chloro-2,3-dihydro-1H-inden-1-OL
CAS No.:3199-71-1
Molecular Formula:C9H9ClO
Molecular Weight:168.623
Hs Code.:2906299090
European Community (EC) Number:863-199-0
DSSTox Substance ID:DTXSID50607366
Mol file:3199-71-1.mol

Synonyms:4-CHLORO-2,3-DIHYDRO-1H-INDEN-1-OL;3199-71-1;4-chloroindan-1-ol;SCHEMBL11110438;DTXSID50607366;IDHGYOQGMVANDO-UHFFFAOYSA-N;AM9282;AKOS010642074;SB84022;DB-305559;EN300-73812;N12836;Z815114596

Suppliers and Price of 4-Chloro-2,3-dihydro-1H-inden-1-OL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
4-Chloro-2,3-dihydro-1H-inden-1-ol 97%
0.5g
$ 146.67

Total 11 raw suppliers

Chemical Property of 4-Chloro-2,3-dihydro-1H-inden-1-OL

Chemical Property:

Vapor Pressure:0.00117mmHg at 25°C
Boiling Point:287.3oC at 760 mmHg
Flash Point:127.5oC
PSA：20.23000
Density:1.322g/cm3
LogP:2.31960
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:168.0341926
Heavy Atom Count:11
Complexity:149

Purity/Quality:

99%, ^*data from raw suppliers

4-Chloro-2,3-dihydro-1H-inden-1-ol 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C1O)C=CC=C2Cl

Technology Process of 4-Chloro-2,3-dihydro-1H-inden-1-OL

There total 7 articles about 4-Chloro-2,3-dihydro-1H-inden-1-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 15115-59-0
4-chloro-2,3-dihydro-1H-inden-1-one

: 3199-71-1
4-chloro-2,3-dihydro-1H-inden-1-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;
DOI:10.1021/jm061475p

Reference yield:

: 83-33-0
inden-1-one

: 3199-71-1
4-chloro-2,3-dihydro-1H-inden-1-ol

Guidance literature:: With hydrogenchloride; sodium borohydrid; In ethanol;

Reference yield:

: 24393-51-9
(E)-ethyl 2-chlorocinnamate

: 3199-71-1
4-chloro-2,3-dihydro-1H-inden-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / H₂ / 5percent Pd/C / ethyl acetate / 3 h

2: 94 percent / KOH / ethanol; H₂O / 4 h / Ambient temperature

3: 1.) SOCl₂, 2.) AlCl₃ / 1.) reflux, 12 h; 2.) CH₂Cl₂, RT, 4 h

4: NaBH₄ / methanol / 2 h

With potassium hydroxide; sodium tetrahydroborate; aluminium trichloride; thionyl chloride; hydrogen; palladium on activated charcoal; In methanol; ethanol; water; ethyl acetate;
DOI:10.1016/S0040-4020(01)91335-3