Ethanone, 1-[2,4-dihydroxy-3-iodo-6-(methoxymethoxy)phenyl]-

Base Information

Chemical Name:Ethanone, 1-[2,4-dihydroxy-3-iodo-6-(methoxymethoxy)phenyl]-
CAS No.:321569-79-3
Molecular Formula:C10H11IO5
Molecular Weight:338.099
Hs Code.:
DSSTox Substance ID:DTXSID70459627
Nikkaji Number:J2.096.048E
Wikidata:Q82283447

Synonyms:321569-79-3;Ethanone, 1-[2,4-dihydroxy-3-iodo-6-(methoxymethoxy)phenyl]-;DTXSID70459627;2',4'-Dihydroxy-3'-iodo-6'-(methoxymethoxy)acetophenone

Suppliers and Price of Ethanone, 1-[2,4-dihydroxy-3-iodo-6-(methoxymethoxy)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Ethanone, 1-[2,4-dihydroxy-3-iodo-6-(methoxymethoxy)phenyl]-

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:337.96512
Heavy Atom Count:16
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=C(C=C(C(=C1O)I)O)OCOC

Technology Process of Ethanone, 1-[2,4-dihydroxy-3-iodo-6-(methoxymethoxy)phenyl]-

There total 3 articles about Ethanone, 1-[2,4-dihydroxy-3-iodo-6-(methoxymethoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 71386-98-6
2',4'-dihydroxy-6'-(methoxymethoxy)acetophenone

: 321569-79-3
2',4'-dihydroxy-3'-iodo-6'-(methoxymethoxy)acetophenone

Guidance literature:: With iodine; periodic acid; In ethanol; water; at 45 ℃; for 0.0333333h; microwave irradiation;
DOI:10.1016/j.tet.2006.06.066

Reference yield:

: 67052-53-3
4',6'-bis(benzyloxy)-2'-(methoxymethoxy)acetophenone

: 321569-79-3
2',4'-dihydroxy-3'-iodo-6'-(methoxymethoxy)acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / hydrogen / palladium on carbon / methanol; ethyl acetate / 20 °C

2: 94 percent / iodine; periodic acid / ethanol / 1 h / 40 °C

With hydrogen; iodine; periodic acid; palladium on activated charcoal; In methanol; ethanol; ethyl acetate;
DOI:10.1080/00397910500514121

Reference yield:

: 18065-05-9
1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

: 321569-79-3
2',4'-dihydroxy-3'-iodo-6'-(methoxymethoxy)acetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / Pd/C / methanol; ethyl acetate / 20 °C

2: 96 percent / I₂; periodic acid / ethanol; H₂O / 0.03 h / 45 °C / microwave irradiation

With hydrogen; iodine; periodic acid; palladium on activated charcoal; In methanol; ethanol; water; ethyl acetate;
DOI:10.1016/j.tet.2006.06.066