Phosphonic acid, [(1-naphthalenylamino)phenylmethyl]-, dimethyl ester

Base Information

• Chemical Name: Phosphonic acid, [(1-naphthalenylamino)phenylmethyl]-, dimethyl ester
• CAS No.: 32394-82-4
• Molecular Formula: C19H20NO3P
• Molecular Weight: 341.346
• Mol file: 32394-82-4.mol

Synonyms:

Chemical Property of Phosphonic acid, [(1-naphthalenylamino)phenylmethyl]-, dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphonic acid, [(1-naphthalenylamino)phenylmethyl]-, dimethyl ester

There total 3 articles about Phosphonic acid, [(1-naphthalenylamino)phenylmethyl]-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-amino-naphthalene (134-32-7) + benzaldehyde (100-52-7) + Dimethyl phosphite (868-85-9) → (±)-dimethyl-[α-(phenyl)(napthalen-1-ylamino)methyl]phosphonate (32394-82-4)

Guidance literature:

With silica supported 20percent dodecatungstophosphoric acid; In acetonitrile; at 20 ℃; for 1h; Green chemistry;

DOI:10.1039/c3ra45853a

Reference yield: 90.0%

1-naphthaldehyde (66-77-3) + Dimethyl phosphite (868-85-9) + aniline (62-53-3) → (±)-dimethyl-[α-(phenyl)(napthalen-1-ylamino)methyl]phosphonate (32394-82-4)

Guidance literature:

With sulfated zirconia supported on magnetic nanoparticles; In neat (no solvent); at 80 ℃; for 0.5h;

DOI:10.1039/c5ra13173a

Reference yield:

→ (±)-dimethyl-[α-(phenyl)(napthalen-1-ylamino)methyl]phosphonate (32394-82-4)

Guidance literature:

entspr. Azomethin, Dimethylhydrogenphosphit;

upstream raw materials:

1-amino-naphthalene

benzaldehyde

Dimethyl phosphite

1-naphthaldehyde