Methanesulfonic acid, trifluoro-, 3-aminophenyl ester

Base Information

Chemical Name:Methanesulfonic acid, trifluoro-, 3-aminophenyl ester
CAS No.:32578-28-2
Molecular Formula:C7H6F3NO3S
Molecular Weight:241.191
Hs Code.:

Synonyms:Methanesulfonic acid,trifluoro-,3-aminophenyl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid, trifluoro-, 3-aminophenyl ester

Chemical Property:

Boiling Point:315.2±42.0 °C(Predicted)
PSA：77.77000
Density:1.574±0.06 g/cm3(Predicted)
LogP:3.15920

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanesulfonic acid, trifluoro-, 3-aminophenyl ester

There total 6 articles about Methanesulfonic acid, trifluoro-, 3-aminophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 591-27-5
m-Hydroxyaniline

: 32578-28-2
(3-Aminophenyl)-trifluormethansulfonat

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.joc.1c02251

Reference yield: 67.0%

: 335-05-7
Trifluoromethanesulfonyl fluoride

: 36309-43-0
3-((trimethylsilyl)oxy)aniline

: 420-56-4
trimethylsilyl fluoride

: 32578-28-2
(3-Aminophenyl)-trifluormethansulfonat

Guidance literature:: triethylamine; In neat (no solvent); in presence of a few HF, CsF, KF, (R4N)F, (C2H5)2NH, effectless in presence of pyridinp, NaF and NH4F;