Ethyl 3-Methyl-5-oxo-[1,3]thiazolo[3,2-a]pyriMidine-6-carboxylate

Base Information

• Chemical Name: Ethyl 3-Methyl-5-oxo-[1,3]thiazolo[3,2-a]pyriMidine-6-carboxylate
• CAS No.: 6124-13-6
• Molecular Formula: C10H10N2O3S
• Molecular Weight: 238.263
• Hs Code.: 2934100090
• Mol file: 6124-13-6.mol

Synonyms:3-Methyl-4-oxo-4H-<1,3>thiazolo<3,2-a>pyrimidin-6-carbonsaeure-aethylester;

Chemical Property of Ethyl 3-Methyl-5-oxo-[1,3]thiazolo[3,2-a]pyriMidine-6-carboxylate

Chemical Property:

• Vapor Pressure: 1.32E-05mmHg at 25°C
• Boiling Point: 368°Cat760mmHg
• Flash Point: 176.3°C
• PSA: 88.91000
• Density: 1.43g/cm³
• LogP: 1.24110

Purity/Quality:

NLT 98% ^*data from raw suppliers

Ethyl3-methyl-5-oxo-[1,3]thiazolo[3,2-a]pyrimidine-6-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 3-Methyl-5-oxo-[1,3]thiazolo[3,2-a]pyriMidine-6-carboxylate

There total 3 articles about Ethyl 3-Methyl-5-oxo-[1,3]thiazolo[3,2-a]pyriMidine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methylthiazol-2-ylamine (1603-91-4) + diethyl 2-ethoxymethylenemalonate (87-13-8) → 3-Methyl-4-oxo-4H-<1,3>thiazolo<3,2-a>pyrimidin-6-carbonsaeure-aethylester (6124-13-6)

Guidance literature:

DOI:10.1021/jo01088a014

Reference yield:

[(4-methyl-thiazol-2-ylamino)-methylene]-malonic acid diethyl ester (6124-09-0) → 3-Methyl-4-oxo-4H-<1,3>thiazolo<3,2-a>pyrimidin-6-carbonsaeure-aethylester (6124-13-6)

Guidance literature:

at 200 - 215 ℃;

Reference yield:

diethyl 2-ethoxymethylenemalonate (87-13-8) → 3-Methyl-4-oxo-4H-<1,3>thiazolo<3,2-a>pyrimidin-6-carbonsaeure-aethylester (6124-13-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 200 - 215 °C

upstream raw materials:

4-methylthiazol-2-ylamine

diethyl 2-ethoxymethylenemalonate

[(4-methyl-thiazol-2-ylamino)-methylene]-malonic acid diethyl ester

Downstream raw materials:

3-methyl-5-oxo-5H-thiazolo[3,2-a]pyrimidine-6-carboxylic acid

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