Methanone, [4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]phenyl-

Base Information

Chemical Name:Methanone, [4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]phenyl-
CAS No.:33809-30-2
Molecular Formula:C17H22O
Molecular Weight:242.361
Hs Code.:
DSSTox Substance ID:DTXSID20466947
Nikkaji Number:J2.480.715K

Synonyms:33809-30-2;Methanone, [4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]phenyl-;DTXSID20466947;(4-tert-butyl-1-cyclohexenyl)-phenylmethanone;(4-tert-butyl-1-cyclohexen-1-yl)(phenyl)methanone

Suppliers and Price of Methanone, [4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, [4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]phenyl-

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:242.167065321
Heavy Atom Count:18
Complexity:326

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1CCC(=CC1)C(=O)C2=CC=CC=C2

Technology Process of Methanone, [4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]phenyl-

There total 9 articles about Methanone, [4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 455-32-3
benzoyl fluoride

: 77412-96-5
1-trifluoromethanesulfonyloxy-4-t-butylcyclohexene

: 33809-30-2
(4-(tert-butyl)cyclohex-1-en-1-yl)(phenyl)methanone

Guidance literature:: With manganese; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; In N,N-dimethyl acetamide; toluene; at 70 ℃; for 15h; Sealed tube;
DOI:10.1021/acs.orglett.9b01164

Reference yield: 80.0%

: 64936-41-0
4-tert-butyl-1-(hydroxy(phenyl)methyl)-1-cyclohexene

: 33809-30-2
(4-(tert-butyl)cyclohex-1-en-1-yl)(phenyl)methanone

Guidance literature:: With 1,10-Phenanthroline; oxygen; potassium carbonate; copper(l) chloride; In benzene; for 2h; Heating;
DOI:10.1016/0040-4020(80)87017-7

Reference yield: 70.0%

: 201230-82-2
carbon monoxide

: 77412-96-5
1-trifluoromethanesulfonyloxy-4-t-butylcyclohexene

: 33809-30-2
(4-(tert-butyl)cyclohex-1-en-1-yl)(phenyl)methanone

Guidance literature:: PhX (X = Li or MgBr); With indium(III) chloride; In tetrahydrofuran; at -78 - 20 ℃;

carbon monoxide; 1-trifluoromethanesulfonyloxy-4-t-butylcyclohexene; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 70 ℃; for 3h; under 1900 Torr;