N-2-methyl-3-pyridinyl-acetamide

Base Information

• Chemical Name: N-2-methyl-3-pyridinyl-acetamide
• CAS No.: 34050-39-0
• Molecular Formula: C8H10N2O
• Molecular Weight: 150.17800
• Hs Code.: 2933399090
• Mol file: 34050-39-0.mol

Synonyms:2-Methyl-3-acetylaminopyridin;3-Acetamido-2-methylpyridin;N-(2-methylpyridin-3-yl)acetamide;N-(2-Methyl-pyridin-3-yl)-acetamide;

Chemical Property of N-2-methyl-3-pyridinyl-acetamide

Chemical Property:

• PSA: 41.99000
• LogP: 1.42140
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

N-(2-Methylpyridin-3-yl)acetamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-2-methyl-3-pyridinyl-acetamide

There total 3 articles about N-2-methyl-3-pyridinyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-3-nitropyridine (18699-87-1) + acetic anhydride (108-24-7) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → N-(2-methyl-pyridin-3-yl)-acetamide (34050-39-0) + 1-(1H-pyrrolo[3,2-b]pyridin-1-yl)ethanone (24509-73-7)

Guidance literature:

2-methyl-3-nitropyridine; N,N-dimethyl-formamide dimethyl acetal; In N,N-dimethyl-formamide; at 120 ℃; for 17h;

With palladium 10% on activated carbon; hydrogen; In methanol; formic acid; for 23h;

acetic anhydride; With dmap; triethylamine; In dichloromethane;

DOI:10.1021/ol900150u

Reference yield:

2-methyl-3-pyridinamine (3430-10-2) + acetic anhydride (108-24-7) → N-(2-methyl-pyridin-3-yl)-acetamide (34050-39-0)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

→ N-(2-methyl-pyridin-3-yl)-acetamide (34050-39-0)

Guidance literature:

2-Methyl-3-aminopyridin, Acetanhydrid;

upstream raw materials:

2-methyl-3-pyridinamine

acetic anhydride

2-methyl-3-nitropyridine

N,N-dimethyl-formamide dimethyl acetal

Downstream raw materials:

1-(1H-pyrazolo[4,3-b]pyridin-1-yl)-ethan-1-one

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