3-Buten-2-one, 3,4-diphenyl-, oxime

Base Information

Chemical Name:3-Buten-2-one, 3,4-diphenyl-, oxime
CAS No.:3475-29-4
Molecular Formula:C16H15NO
Molecular Weight:237.301
Hs Code.:

Synonyms:

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Chemical Property of 3-Buten-2-one, 3,4-diphenyl-, oxime

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3-Buten-2-one, 3,4-diphenyl-, oxime

There total 10 articles about 3-Buten-2-one, 3,4-diphenyl-, oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1722-69-6
3,4-diphenylbut-3-en-2-one

: 3475-29-4
3,4-diphenyl-but-3-en-2-one oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In methanol; water; at 65 ℃; for 1h;
DOI:10.1039/c4nj02075h

Reference yield:

: 54963-40-5
(Z)-3,4-diphenyl-3-buten-2-one

: C₁₆H₁₅NO

: 1721-85-3,3475-29-4,21736-65-2,21736-66-3,73151-58-3
trans-1,2-Diphenyl-but-1-en-3-on-syn(methyl)-oxim

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol202176g

Reference yield:

: 591-50-4
iodobenzene

: C₁₆H₁₅NO

: 1721-85-3,3475-29-4,21736-65-2,21736-66-3,73151-58-3
trans-1,2-Diphenyl-but-1-en-3-on-syn(methyl)-oxim

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 5 h / 20 °C / Inert atmosphere

2: [Rh(OH)(cod)]2; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane; water / 3 h / 20 - 60 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

4: hydroxylamine hydrochloride; sodium acetate / methanol / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; [Rh(OH)(cod)]2; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; Dess-Martin periodane; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; 1: Sonogashira coupling;
DOI:10.1021/ol202176g