2-(4-Nitrophenyl)-3-phenyl-1H-inden-1-one

Base Information

Chemical Name:2-(4-Nitrophenyl)-3-phenyl-1H-inden-1-one
CAS No.:3513-39-1
Molecular Formula:C₂₁H₁₃NO₃
Molecular Weight:327.339
Hs Code.:
DSSTox Substance ID:DTXSID20538890
Nikkaji Number:J2.982.588B
Wikidata:Q82414462
Mol file:3513-39-1.mol

Synonyms:3513-39-1;2-(4-Nitrophenyl)-3-phenyl-1H-inden-1-one;DTXSID20538890

Suppliers and Price of 2-(4-Nitrophenyl)-3-phenyl-1H-inden-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(4-Nitrophenyl)-3-phenyl-1H-inden-1-one

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:327.08954328
Heavy Atom Count:25
Complexity:562

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C(=O)C3=CC=CC=C32)C4=CC=C(C=C4)[N+](=O)[O-]

Technology Process of 2-(4-Nitrophenyl)-3-phenyl-1H-inden-1-one

There total 5 articles about 2-(4-Nitrophenyl)-3-phenyl-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1942-30-9
4-(phenylethynyl)nitrobenzene

: 6630-33-7
ortho-bromobenzaldehyde

: 3-(4-nitrophenyl)-2-phenyl-1H-inden-1-one

: 3513-39-1
2-(4-nitrophenyl)-3-phenyl-1H-inden-1-one

Guidance literature:: With [Pd((η5-C5H5)Fe[(η5-C5H3)C(Me)=N(C6H4-4-Me)])ClPPh3]; tetrabutylammomium bromide; potassium carbonate; benzoic acid; In N,N-dimethyl-formamide; at 110 ℃; for 4h; Inert atmosphere;
DOI:10.1002/aoc.1826

Reference yield:

: 1942-30-9
4-(phenylethynyl)nitrobenzene

: 5159-41-1
2-iodobenzyl alcohol

: 3-(4-nitrophenyl)-2-phenyl-1H-inden-1-one

: 3513-39-1
2-(4-nitrophenyl)-3-phenyl-1H-inden-1-one

Guidance literature:: With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); oxygen; potassium carbonate; In water; at 70 ℃; for 24h; Overall yield = 83 %; Overall yield = 135 mg; regioselective reaction; Green chemistry;
DOI:10.1021/jo501444g

Reference yield:

: 1801-42-9
2,3-diphenyl-1H-inden-1-one

: 3513-39-1
2-(4-nitrophenyl)-3-phenyl-1H-inden-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; HNO₃ / Beim anschliessenden Behandeln mit H₂O

With nitric acid; acetic acid;