[(2-Chloro-2-propenyl)oxy]benzene

Base Information

• Chemical Name: [(2-Chloro-2-propenyl)oxy]benzene
• CAS No.: 53299-53-9
• Molecular Formula: C9H9ClO
• Molecular Weight: 168.623
• Hs Code.: 2909309090
• Mol file: 53299-53-9.mol

Synonyms:(2-chloro-allyl)-phenyl ether;Benzene,[(2-chloro-2-propenyl)oxy];2-Chlor-3-phenoxy-propen-(1);[(2-Chloro-2-propenyl)oxy]benzene;3-Aryloxy-2-chloropropen;(2-Chlor-allyl)-phenyl-aether;Chloroallylphenylether;Benzene, [(2-chloro-2-propenyl)oxy]-;

Chemical Property of [(2-Chloro-2-propenyl)oxy]benzene

Chemical Property:

• Vapor Pressure: 0.0615mmHg at 25°C
• Boiling Point: 239.6°Cat760mmHg
• Flash Point: 103.3°C
• PSA: 9.23000
• Density: 1.104g/cm³
• LogP: 2.81790

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [(2-Chloro-2-propenyl)oxy]benzene

There total 4 articles about [(2-Chloro-2-propenyl)oxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,3-Dichloroprop-1-ene (78-88-6) + phenol (108-95-2,27073-41-2) → 2-chloro-3-phenoxyprop-1-ene (53299-53-9)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 95 - 105 ℃; for 4h;

Reference yield: 84.0%

1,2,3-trichloropropane (96-18-4) + phenol (108-95-2,27073-41-2) → 2-chloro-3-phenoxyprop-1-ene (53299-53-9)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 95 - 105 ℃; for 4h; Product distribution; other temperatures, other reaction times, other alkylphenols, other 1,2,3-trihalogenpropane;

Reference yield:

1,2,3-trichloropropane (96-18-4) + sodium phenoxide (139-02-6) → 2-chloro-3-phenoxyprop-1-ene (53299-53-9)

Guidance literature:

In dimethyl sulfoxide;

DOI:10.1246/bcsj.49.1931

upstream raw materials:

2,3-Dichloroprop-1-ene

phenol

1,2,3-trichloropropane

sodium phenoxide

Downstream raw materials:

2-(2-chloro-allyl)-phenol

2-methylbenzofuran