2-Hexenoic acid, 5-hydroxy-5-phenyl-, (E)-

Base Information

Chemical Name:2-Hexenoic acid, 5-hydroxy-5-phenyl-, (E)-
CAS No.:35490-01-8
Molecular Formula:C₁₂H₁₄O₃
Molecular Weight:206.241
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Hexenoic acid, 5-hydroxy-5-phenyl-, (E)-

Chemical Property:

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Technology Process of 2-Hexenoic acid, 5-hydroxy-5-phenyl-, (E)-

There total 4 articles about 2-Hexenoic acid, 5-hydroxy-5-phenyl-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (+/-)-5-hydroxy-5-phenyl-hex-2t-enoic acid tert-butyl ester

: 35490-01-8
(+/-)-5-hydroxy-5-phenyl-hex-2t-enoic acid

Guidance literature:: With 1,4-dioxane; hydrogenchloride;
DOI:10.1021/ja01101a016

Reference yield:

: 98-86-2
acetophenone

: 35490-01-8
(+/-)-5-hydroxy-5-phenyl-hex-2t-enoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: LiNH₂

2: concentrated aqueous HCl; dioxane

With 1,4-dioxane; hydrogenchloride; lithium amide;
DOI:10.1021/ja01101a016

Reference yield:

: acide γ-bromocrotonique

: 106-95-6
allyl bromide

: 98-86-2
acetophenone

: 35490-01-8
(+/-)-5-hydroxy-5-phenyl-hex-2t-enoic acid

: 69637-34-9
2-(1-hydroxy-1-phenylethyl)-but-3-enoic acid

Guidance literature:: With zinc; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, 0 deg C; 2.) THF, reflux, 4 h;
DOI:10.1016/S0040-4020(01)96531-7