2-Oxazolidinone, 3-[(2S,3E)-2-[(1S,2R)-1-hydroxy-2-[(4-methoxyphenyl)methoxy]-3-buten yl]-3,7-dimethyl-1-oxo-3,6-octadienyl]-4-(phenylmethyl)-, (4R)-

Base Information

Chemical Name:2-Oxazolidinone, 3-[(2S,3E)-2-[(1S,2R)-1-hydroxy-2-[(4-methoxyphenyl)methoxy]-3-buten yl]-3,7-dimethyl-1-oxo-3,6-octadienyl]-4-(phenylmethyl)-, (4R)-
CAS No.:364337-21-3
Molecular Formula:C32H39NO6
Molecular Weight:533.665
Hs Code.:

2-Oxazolidinone,
3-[(2S,3E)-2-[(1S,2R)-1-hydroxy-2-[(4-methoxyphenyl)methoxy]-3-buten
yl]-3,7-dimethyl-1-oxo-3,6-octadienyl]-4-(phenylmethyl)-, (4R)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Oxazolidinone, 3-[(2S,3E)-2-[(1S,2R)-1-hydroxy-2-[(4-methoxyphenyl)methoxy]-3-buten yl]-3,7-dimethyl-1-oxo-3,6-octadienyl]-4-(phenylmethyl)-, (4R)-

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Technology Process of 2-Oxazolidinone, 3-[(2S,3E)-2-[(1S,2R)-1-hydroxy-2-[(4-methoxyphenyl)methoxy]-3-buten yl]-3,7-dimethyl-1-oxo-3,6-octadienyl]-4-(phenylmethyl)-, (4R)-

There total 10 articles about 2-Oxazolidinone, 3-[(2S,3E)-2-[(1S,2R)-1-hydroxy-2-[(4-methoxyphenyl)methoxy]-3-buten yl]-3,7-dimethyl-1-oxo-3,6-octadienyl]-4-(phenylmethyl)-, (4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1054617-67-2
(R)-4-Benzyl-3-{(E)-(S)-2-[(1S,2R)-1-hydroxy-2-(4-methoxy-benzyloxy)-4-phenylselanyl-butyl]-3,7-dimethyl-octa-3,6-dienoyl}-oxazolidin-2-one

: 364337-21-3
(4R)-4-benzyl-3-{(2S)-2-[(1S,2R)-1-hydroxy-2-p-methoxybenzyloxy-but-3-enyl]-3,7-dimethyloct-3,6-dienoyl}-oxazolidin-2-one

Guidance literature:: With tetrabutylammonium periodite; In chloroform; at 60 ℃; for 2h;
DOI:10.1021/ol016343z

Reference yield:

: 16750-94-0
2,6-dimethyl-2,5-octadien-8-ol

: 364337-21-3
(4R)-4-benzyl-3-{(2S)-2-[(1S,2R)-1-hydroxy-2-p-methoxybenzyloxy-but-3-enyl]-3,7-dimethyloct-3,6-dienoyl}-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: 35 percent / CrO₃; sulfuric acid / H₂O; acetone / 0.25 h / 0 °C

2.1: triethylamine / tetrahydrofuran / 0.5 h / -78 - 0 °C

3.1: 188 mg / tetrahydrofuran; hexane / 0.33 h / -78 °C

4.1: LDA / tetrahydrofuran; hexane / 0.75 h / -78 °C

4.2: tetrahydrofuran; hexane / 0.75 h / -78 °C

5.1: 4.61 g / tetrabutylammonium periodate / CHCl₃ / 2 h / 60 °C

With chromium(VI) oxide; sulfuric acid; tetrabutylammonium periodite; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; chloroform; water; acetone;
DOI:10.1021/ol016343z

Reference yield:

: 372504-89-7
(R)-4-benzyl-2-oxazolidinone lithium salt

: 364337-21-3
(4R)-4-benzyl-3-{(2S)-2-[(1S,2R)-1-hydroxy-2-p-methoxybenzyloxy-but-3-enyl]-3,7-dimethyloct-3,6-dienoyl}-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: 188 mg / tetrahydrofuran; hexane / 0.33 h / -78 °C

2.1: LDA / tetrahydrofuran; hexane / 0.75 h / -78 °C

2.2: tetrahydrofuran; hexane / 0.75 h / -78 °C

3.1: 4.61 g / tetrabutylammonium periodate / CHCl₃ / 2 h / 60 °C

With tetrabutylammonium periodite; lithium diisopropyl amide; In tetrahydrofuran; hexane; chloroform;
DOI:10.1021/ol016343z