Isoxazole, 4-(4-methoxyphenyl)-3,5-diphenyl-

Base Information

Chemical Name:Isoxazole, 4-(4-methoxyphenyl)-3,5-diphenyl-
CAS No.:365212-54-0
Molecular Formula:C22H17NO2
Molecular Weight:327.382
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Isoxazole, 4-(4-methoxyphenyl)-3,5-diphenyl-

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Technology Process of Isoxazole, 4-(4-methoxyphenyl)-3,5-diphenyl-

There total 5 articles about Isoxazole, 4-(4-methoxyphenyl)-3,5-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 622-42-4
1-nitro-1-phenylmethane

: 123-11-5
4-methoxy-benzaldehyde

: 365212-54-0
3,5-diphenyl-4-(4-methoxyphenyl)isoxazole

Guidance literature:: With aluminum oxide; at 140 ℃; for 3h; microwave irradiation;
DOI:10.1080/00304940109356606

Reference yield: 68.0%

: 850131-31-6
3,5-diphenyl-4-(dimethylhydroxysilyl)isoxazole

: 696-62-8
para-iodoanisole

: 365212-54-0
3,5-diphenyl-4-(4-methoxyphenyl)isoxazole

Guidance literature:: With sodium t-butanolate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In 1,4-dioxane; at 80 ℃; for 4h;
DOI:10.1021/jo047755z

Reference yield:

: 87710-79-0
methoxy-dimethyl(phenylethynyl)silane

: 365212-54-0
3,5-diphenyl-4-(4-methoxyphenyl)isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: KHCO₃ / dioxane / 4.5 h / Heating

1.2: 52 percent / AcOH / acetonitrile; H₂O / 1.25 h / 20 °C

2.1: 68 percent / t-BuONa / Pd₂(dba)3*CHCl₃ / dioxane / 4 h / 80 °C

With potassium hydrogencarbonate; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In 1,4-dioxane;
DOI:10.1021/jo047755z