Carbamic acid, [(1S,2R)-2-azidocyclohexyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S,2R)-2-azidocyclohexyl]-, 1,1-dimethylethyl ester
CAS No.:365996-29-8
Molecular Formula:C11H20N4O2
Molecular Weight:240.305
Hs Code.:
Mol file:365996-29-8.mol

Synonyms:Carbamic acid,N-[(1S,2R)-2-azidocyclohexyl]-,1,1-dimethylethyl ester;D-1328;

Suppliers and Price of Carbamic acid, [(1S,2R)-2-azidocyclohexyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Carbamic acid, [(1S,2R)-2-azidocyclohexyl]-, 1,1-dimethylethyl ester

Chemical Property:

Melting Point:69-70 °C
PSA：91.57000
LogP:2.78976

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(1S,2R)-2-azidocyclohexyl]-, 1,1-dimethylethyl ester

There total 16 articles about Carbamic acid, [(1S,2R)-2-azidocyclohexyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 365996-28-7
(1S,2S)-2-(tert-butoxycarbonylamino)cyclohexyl methanesulfonate

: 365996-29-8
(1R,2S)-2-(N-tert-butyloxycarbonylamino)-1-azidocyclohexane

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 90 ℃; for 0.133333h; microwave irradiation;

Reference yield: 87.0%

: 365996-28-7
(1S,2S)-2-(tert-butoxycarbonylamino)cyclohexyl methanesulfonate

: 875923-28-7
(3aRS,7aSR)-octahydro-2H-benzimidazol-2-one

: 365996-29-8
(1R,2S)-2-(N-tert-butyloxycarbonylamino)-1-azidocyclohexane

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; for 12h; Heating;

Reference yield:

: 931-15-7,931-16-8,6850-38-0,6982-39-4,33092-82-9,38898-70-3,74111-21-0,108267-20-5
(1S,2S)-trans-2-aminocyclohexanol

: 365996-29-8
(1R,2S)-2-(N-tert-butyloxycarbonylamino)-1-azidocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂

2: 94 percent / pyridine

3: 47 percent / NaN₃ / dimethylformamide

With pyridine; sodium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.05.068