1,1-Diphenyl-N-(pyridin-2-yl)methanimine

Base Information

• Chemical Name: 1,1-Diphenyl-N-(pyridin-2-yl)methanimine
• CAS No.: 36728-56-0
• Molecular Formula: C18H14N2
• Molecular Weight: 258.323
• DSSTox Substance ID: DTXSID20538855
• Mol file: 36728-56-0.mol

Synonyms:36728-56-0;1,1-Diphenyl-N-(pyridin-2-yl)methanimine;SCHEMBL2729935;DTXSID20538855

Chemical Property of 1,1-Diphenyl-N-(pyridin-2-yl)methanimine

Chemical Property:

• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 258.115698455
• Heavy Atom Count: 20
• Complexity: 291

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NC2=CC=CC=N2)C3=CC=CC=C3

Technology Process of 1,1-Diphenyl-N-(pyridin-2-yl)methanimine

There total 3 articles about 1,1-Diphenyl-N-(pyridin-2-yl)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-chloropyridine (109-09-1) + Benzophenone imine (1013-88-3) → N-(2-pyridinyl)benzophenone imine (36728-56-0)

Guidance literature:

With sodium t-butanolate; In toluene; at 100 - 110 ℃; for 18h; Inert atmosphere; Sealed vial;

DOI:10.1002/chem.200902316

Reference yield: 30.0%

2-aminopyridine (504-29-0) + dimethoxydiphenylmethane (2235-01-0) → N-(2-pyridinyl)benzophenone imine (36728-56-0)

Guidance literature:

at 200 ℃; for 96h;

Reference yield:

α,α'-Diphenyl-2-pyridylazidomethane → N-(phenyl(pyridin-2-yl)methylene)aniline (30894-24-7) + N-(2-pyridinyl)benzophenone imine (36728-56-0)

Guidance literature:

In dodecane; at 200 ℃; for 0.5h; Product distribution; Mechanism; other solvent (nitrobenzene), migration aptitude, conversion rate;

upstream raw materials:

2-aminopyridine

dimethoxydiphenylmethane

2-chloropyridine

Benzophenone imine