2-Propenoic acid, 2-(diethoxyphosphinyl)-3-(4-methoxyphenyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-

Base Information

• Chemical Name: 2-Propenoic acid, 2-(diethoxyphosphinyl)-3-(4-methoxyphenyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-
• CAS No.: 367911-54-4
• Molecular Formula: C₃₀H₄₁O₆P
• Molecular Weight: 528.626
• Mol file: 367911-54-4.mol

Synonyms:

Chemical Property of 2-Propenoic acid, 2-(diethoxyphosphinyl)-3-(4-methoxyphenyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-

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Technology Process of 2-Propenoic acid, 2-(diethoxyphosphinyl)-3-(4-methoxyphenyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-

There total 2 articles about 2-Propenoic acid, 2-(diethoxyphosphinyl)-3-(4-methoxyphenyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzaldehyde (123-11-5) + (diethoxyphosphoryl)acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester (155795-48-5) → (-)-8-phenylmenthyl (Z)-2-(diethoxyphosphoryl)-3-(4-methoxyphenyl)acrylate (367911-54-4)

Guidance literature:

With triisopropoxytitanium(IV) chloride; triethylamine; In tetrahydrofuran; at -78 ℃;

DOI:10.1016/S0040-4039(01)01116-9

Reference yield:

4-methoxy-benzaldehyde (123-11-5) + (diethoxyphosphoryl)acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester (155795-48-5) → (-)-8-phenylmenthyl (E)-2-(diethoxyphosphoryl)-3-(4-methoxyphenyl)acrylate (367911-51-1) + (-)-8-phenylmenthyl (Z)-2-(diethoxyphosphoryl)-3-(4-methoxyphenyl)acrylate (367911-54-4)

Guidance literature:

With 4-methyl-morpholine; titanium tetrachloride; In tetrahydrofuran; tetrachloromethane; at 0 ℃; for 3h;

Reference yield:

trimethylsulfoxonium iodide (1774-47-6) + (-)-8-phenylmenthyl (Z)-2-(diethoxyphosphoryl)-3-(4-methoxyphenyl)acrylate (367911-54-4) → (-)-8-phenylmenthyl cis-1-(diethoxyphosphoryl)-2-(4-methoxyphenyl)cyclopropanecarboxylate + (+)-8-phenylmenthyl trans-1-(diethoxyphosphoryl)-2-(4-methoxyphenyl)cyclopropanecarboxylate + (-)-8-phenylmenthyl trans-1-(diethoxyphosphoryl)-2-(4-methoxyphenyl)cyclopropanecarboxylate + (+)-8-phenylmenthyl cis-1-(diethoxyphosphoryl)-2-(4-methoxyphenyl)cyclopropanecarboxylate

Guidance literature:

With sodium hydride; In dimethyl sulfoxide; at 25 ℃;

DOI:10.1016/S0040-4039(01)01116-9

upstream raw materials:

4-methoxy-benzaldehyde

(diethoxyphosphoryl)acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester

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