1,6-difluorohexane

Base Information

• Chemical Name: 1,6-difluorohexane
• CAS No.: 373-29-5
• Molecular Formula: C6H12F2
• Molecular Weight: 122.158
• Hs Code.: 2903399090
• Mol file: 373-29-5.mol

Synonyms:1,6-diethoxybenzopyrene;1,6-Difluor-hexan;1,6-difluoro-hexane;

Chemical Property of 1,6-difluorohexane

Chemical Property:

• Refractive Index: 1.3409 (estimate)
• Boiling Point: 117.34°C (rough estimate)
• PSA: 0.00000
• Density: 0.9315 (rough estimate)
• LogP: 2.48580

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-difluorohexane

There total 5 articles about 1,6-difluorohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,6-hexanediol (629-11-8) → oxepane (592-90-5) + 1,6-difluorohexane (373-29-5) + 6-fluoro-hexan-1-ol (373-32-0)

Guidance literature:

With 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; for 0.5h; Yield given. Yields of byproduct given;

Reference yield:

C7H12ClFO2 → 1,6-difluorohexane (373-29-5) + 1-chloro-6-fluorohexane (1550-09-0) + 1,6-dichlorohexane (2163-00-0)

Guidance literature:

With HBGF; at 120 ℃; for 1.5h; Title compound not separated from byproducts;

DOI:10.1016/S0040-4039(02)00738-4

Reference yield:

1,6-dichlorohexane (2163-00-0) → hex-5-enyl fluoride (373-15-9) + 1,6-difluorohexane (373-29-5)

Guidance literature:

With potassium fluoride; ethylene glycol; at 185 ℃;

upstream raw materials:

1,6-dichlorohexane

1,6-hexanediol

ethylene glycol

Downstream raw materials:

1-hexyl-4-methyl-benzene

1,6-di(p-tolyl)hexane

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