2-[(1E)-2-nitroprop-1-en-1-yl]thiophene

Base Information

Chemical Name:2-[(1E)-2-nitroprop-1-en-1-yl]thiophene
CAS No.:37629-59-7
Molecular Formula:C7H7NO2S
Molecular Weight:169.20100
Hs Code.:
Mol file:37629-59-7.mol

Synonyms:2-((E)-2-nitro-propenyl)-thiophene;2-(2-nitropropenyl)thiophene;2-(2-nitropropen-1-yl)thiophene;2-Nitro-1-(2-thienyl)-propen;2-nitro-1-(2-thienyl)propen;1-(2-thienyl)-2-nitropropene;

Suppliers and Price of 2-[(1E)-2-nitroprop-1-en-1-yl]thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-[(1E)-2-nitroprop-1-en-1-yl]thiophene

Chemical Property:

Vapor Pressure:0.00957mmHg at 25°C
PSA：74.06000
LogP:2.90880

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[(1E)-2-nitroprop-1-en-1-yl]thiophene

There total 4 articles about 2-[(1E)-2-nitroprop-1-en-1-yl]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 98-03-3
thiophene-2-carbaldehyde

: 79-24-3
Nitroethane

: 37629-59-7
(E)-2-(2-nitroprop-1-en-1-yl)thiophene

Guidance literature:: With acetic acid; N-butylamine; at 80 ℃; for 2h;
DOI:10.1002/ejoc.201700165

Reference yield: 77.5%

: 37629-59-7
(E)-2-(2-nitroprop-1-en-1-yl)thiophene

Guidance literature:: With formic acid; ethanolamine; for 0.166667h; Cooling with ice;

for 5h; Reflux;

Reference yield:

: C₈H₇F₃O₃S₂

: 37629-59-7
(E)-2-(2-nitroprop-1-en-1-yl)thiophene

Guidance literature:: C₈H₇F₃O₃S₂; With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,2-dimethoxyethane; at 20 ℃; for 0.166667h; Inert atmosphere;

With tetrabutylammomium bromide; sodium nitrite; In 1,2-dimethoxyethane; for 5h; Reflux;
DOI:10.1016/j.tetlet.2013.04.038