Benzene, 1-(3-azidopropyl)-3-fluoro-2-methyl-

Base Information

Chemical Name:Benzene, 1-(3-azidopropyl)-3-fluoro-2-methyl-
CAS No.:377083-83-5
Molecular Formula:C10H12FN3
Molecular Weight:193.224
Hs Code.:

Synonyms:

Suppliers and Price of Benzene, 1-(3-azidopropyl)-3-fluoro-2-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzene, 1-(3-azidopropyl)-3-fluoro-2-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, 1-(3-azidopropyl)-3-fluoro-2-methyl-

There total 5 articles about Benzene, 1-(3-azidopropyl)-3-fluoro-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 377083-82-4
C₁₁H₁₅FO₃S

: 377083-83-5
C₁₀H₁₂FN₃

Guidance literature:: With sodium azide; tetra(n-butyl)ammonium hydrogensulfate; In dimethyl sulfoxide; at 45 ℃; for 16h;

Reference yield:

: 155814-23-6
3-fluoro-2-methylcinnamic acid

: 377083-83-5
C₁₀H₁₂FN₃

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium hydroxide/carbon / ethanol / 22 h

2: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 °C

3: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

4: sodium azide; tetra(n-butyl)ammonium hydrogensulfate / dimethyl sulfoxide / 16 h / 45 °C

With lithium aluminium tetrahydride; sodium azide; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; palladium hydroxide/carbon; In tetrahydrofuran; ethanol; dimethyl sulfoxide;

Reference yield:

: 147624-13-3
3-fluoro-2-methylbenzaldehyde

: 377083-83-5
C₁₀H₁₂FN₃

Guidance literature:: Multi-step reaction with 5 steps

1: piperidine / toluene / 22 h / Heating / reflux

2: hydrogen / palladium hydroxide/carbon / ethanol / 22 h

3: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 °C

4: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

5: sodium azide; tetra(n-butyl)ammonium hydrogensulfate / dimethyl sulfoxide / 16 h / 45 °C

With piperidine; lithium aluminium tetrahydride; sodium azide; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; palladium hydroxide/carbon; In tetrahydrofuran; ethanol; dimethyl sulfoxide; toluene;