1,2-Dichloro-1,1,2-trifluoro-2-iodoethane

Base Information

• Chemical Name: 1,2-Dichloro-1,1,2-trifluoro-2-iodoethane
• CAS No.: 354-61-0
• Molecular Formula: C2Cl2F3I
• Molecular Weight: 278.828
• Hs Code.: 2903799090
• European Community (EC) Number: 206-565-1
• UNII: O8W7U5MNKR
• DSSTox Substance ID: DTXSID70870510
• Nikkaji Number: J193.831B
• Wikidata: Q27285490
• Mol file: 354-61-0.mol

Synonyms:354-61-0;1,2-Dichloro-1,1,2-trifluoro-2-iodoethane;1,2-Dichloro-2-iodo-1,1,2-trifluoroethane;1,2-dichlorotrifluoro-1-iodoethane;1,2-dichloro-1-iodotrifluoroethane;1,2-Dichloro-2-iodotrifluoroethane;EINECS 206-565-1;UNII-O8W7U5MNKR;O8W7U5MNKR;Ethane, 1,2-dichloro-1,1,2-trifluoro-2-iodo-;MFCD00039402;C2Cl2F3I;C2-Cl2-F3-I;1,2-Dichlorotrifluoroiodoethane;SCHEMBL1284179;DTXSID70870510;AKOS005762922;J193.831B;FT-0606369;1,1,2-Trifluoro-1,2-dichloro-2-iodoethane;Q27285490

Chemical Property of 1,2-Dichloro-1,1,2-trifluoro-2-iodoethane

Chemical Property:

• Vapor Pressure: 38.5mmHg at 25°C
• Refractive Index: 1.449
• Boiling Point: 102.7 °C at 760 mmHg
• Flash Point: 15.9 °C
• PSA: 0.00000
• Density: 2.331 g/cm³
• LogP: 3.11510
• Sensitive.: Light Sensitive
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 277.83739
• Heavy Atom Count: 8
• Complexity: 97.3

Purity/Quality:

99% ^*data from raw suppliers

1,2-Dichloro-1,1,2-trifluoro-2-iodoethane, tech ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(F)(Cl)I)(F)(F)Cl

Technology Process of 1,2-Dichloro-1,1,2-trifluoro-2-iodoethane

There total 4 articles about 1,2-Dichloro-1,1,2-trifluoro-2-iodoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Chlorotrifluoroethylene (79-38-9,9036-80-0) → 1,1,2-Trichloro-1,2,2-trifluoroethane (76-13-1) + 1,2-dichloro-1,2,2-trifluoro-1-iodoethane (354-61-0) + 2,2-Dichlorotrifluoro-1-iodoethane (661-66-5)

Guidance literature:

With Iodine monochloride;

DOI:10.1021/jo01051a530

Reference yield:

Chlorotrifluoroethylene (79-38-9,9036-80-0) → 1,1,2-Trichloro-1,2,2-trifluoroethane (76-13-1) + 1,2-dichloro-1,2,2-trifluoro-1-iodoethane (354-61-0)

Guidance literature:

at 35 - 40 ℃; unter Druck;

DOI:10.1039/jr9520004423

Reference yield:

Chlorotrifluoroethylene (79-38-9,9036-80-0) → 1,2-dichloro-1,2,2-trifluoro-1-iodoethane (354-61-0) + 2,2-Dichlorotrifluoro-1-iodoethane (661-66-5)

Guidance literature:

With Iodine monochloride; In dichloromethane; at -8 - -5 ℃;

DOI:10.1021/ja01472a018

upstream raw materials:

Chlorotrifluoroethylene

polytetrafluoroethylene

methyllithium

Downstream raw materials:

1,2-dichloro-dodecafluoro-6-iodo-4-trifluoromethyl-heptane

1,2-dichloro-4-iodo-1,1,2-trifluorobutane

perfluoro-1,2,3,4-tetrachlorobutane

1,2-dichloro-1,1,2,3,3,4,4-heptafluoro-4-iodo-butane

Refernces

• 1、 Bissell,E.R.,Shaw,G.C.. "-". . p. 1482 - 1483. Retrieved 1962.
• 2、 Tayouo, Russell,David, Ghislain,Ameduri, Bruno,Boutevin, Bernard. "Oligomers of vinyl phosphonic acid obtained by radical polymerization in the presence of halogenated chain transfer agent". experimental part. p. 545 - 548. Retrieved 2010/09/04.
• 3、 -. "Perhaloethyl aromatic compounds and perhaloethenyl aromatic compounds therefrom". Page column 4. . Retrieved 2008/06/13.