Cybrodic acid

Base Information

Chemical Name:Cybrodic acid
CAS No.:75225-86-4
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

Synonyms:

Suppliers and Price of Cybrodic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cybrodic acid

Chemical Property:

Purity/Quality:

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Technology Process of Cybrodic acid

There total 11 articles about Cybrodic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74973-56-1
2-(4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 75225-86-4
cybrodic acid

Guidance literature:: Multi-step reaction with 8 steps

1: bromine / nitromethane / 0.5 h / 0 °C

2: 95 percent / pyridinium tosylate / CH₂Cl₂ / 1 h / Ambient temperature

3: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

4: 67 percent / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

5: 100 percent / activated MnO₂ / CH₂Cl₂ / Ambient temperature

6: 95 percent / acetic acid, sodium cyanide, activated MnO₂ / 48 h / Ambient temperature

7: 77 percent / ferric chloride / 2 h / Ambient temperature

8: KOH / H₂O; methanol / 1.5 h / Heating

With sodium cyanide; manganese(IV) oxide; potassium hydroxide; n-butyllithium; sulfuric acid; bromine; pyridinium p-toluenesulfonate; iron(III) chloride; acetic acid; In tetrahydrofuran; methanol; nitromethane; dichloromethane; water; acetone;
DOI:10.1139/v81-311

Reference yield:

: 79801-57-3
2-(3-bromo-4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 75225-86-4
cybrodic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / pyridinium tosylate / CH₂Cl₂ / 1 h / Ambient temperature

2: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

3: 67 percent / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

4: 100 percent / activated MnO₂ / CH₂Cl₂ / Ambient temperature

5: 95 percent / acetic acid, sodium cyanide, activated MnO₂ / 48 h / Ambient temperature

6: 77 percent / ferric chloride / 2 h / Ambient temperature

7: KOH / H₂O; methanol / 1.5 h / Heating

With sodium cyanide; manganese(IV) oxide; potassium hydroxide; n-butyllithium; sulfuric acid; pyridinium p-toluenesulfonate; iron(III) chloride; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1139/v81-311

Reference yield:

: 74973-57-2
1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

: 75225-86-4
cybrodic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

2: 67 percent / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

3: 100 percent / activated MnO₂ / CH₂Cl₂ / Ambient temperature

4: 95 percent / acetic acid, sodium cyanide, activated MnO₂ / 48 h / Ambient temperature

5: 77 percent / ferric chloride / 2 h / Ambient temperature

6: KOH / H₂O; methanol / 1.5 h / Heating

With sodium cyanide; manganese(IV) oxide; potassium hydroxide; n-butyllithium; sulfuric acid; iron(III) chloride; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1139/v81-311