1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

Base Information

Chemical Name:1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene
CAS No.:74973-57-2
Molecular Formula:C₁₇H₂₅BrO₃
Molecular Weight:357.288
Hs Code.:

Synonyms:1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

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Chemical Property of 1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

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Technology Process of 1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

There total 6 articles about 1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 79801-57-3
2-(3-bromo-4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 74973-57-2
1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1139/v81-311

Reference yield:

: 74973-56-1
2-(4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 74973-57-2
1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / nitromethane / 0.5 h / 0 °C

2: 95 percent / pyridinium tosylate / CH₂Cl₂ / 1 h / Ambient temperature

With bromine; pyridinium p-toluenesulfonate; In nitromethane; dichloromethane;
DOI:10.1139/v81-311

Reference yield:

: 576-83-0
2,4,6-trimethylphenyl bromide

: 74973-57-2
1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

Guidance literature:: Multi-step reaction with 6 steps

1: 50 percent

2: LAH

3: NaH

4: 1. butyllithium / 1. THF/hexane, -78 deg C

5: Br₂ / acetonitrile / 0 °C

6: pyridinium tosylate / CH₂Cl₂

With lithium aluminium tetrahydride; n-butyllithium; bromine; pyridinium p-toluenesulfonate; sodium hydride; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)93644-X