trichechol

Base Information

Chemical Name:trichechol
CAS No.:114882-48-3
Molecular Formula:C₂₇H₄₈O₅
Molecular Weight:452.675
Hs Code.:
Mol file:114882-48-3.mol

Synonyms:5b-Cholestane-3a,6b,7a,25,26-pentol

Suppliers and Price of trichechol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of trichechol

Chemical Property:

Vapor Pressure:8.17E-17mmHg at 25°C
Boiling Point:598.4°Cat760mmHg
Flash Point:252°C
PSA：101.15000
Density:1.146g/cm³
LogP:3.49750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of trichechol

There total 14 articles about trichechol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3664-87-7
3α-hydroxy-5β-chol-6-en-24-oic acid

: 114882-48-3
5β-cholestane-3α,6β,7α,25,26-pentol

Guidance literature:: Multi-step reaction with 13 steps

1: 4 h / 55 °C

2: SOCl₂ / 2 h / Ambient temperature

3: diethyl ether

4: collidine / 0.25 h / 180 - 200 °C

5: 10percent KOH in MeOH / 1 h / Heating

6: diethyl ether / 2 h

7: 1) m-chloroperbenzoic acid, 2) AcOH / 1) CHCl₃, 24 h, RT, 2) reflux, 3.5 h

8: 5percent KOH in MeOH / 1 h / Heating

9: NaOAc / 100 °C / Heating

10: SOCl₂

11: diethyl ether / Ambient temperature

12: 24 h / Ambient temperature

13: diethyl ether / 1) reflux, 2.5 h, 2) RT, overnight

With 2,3,5-trimethyl-pyridine; potassium hydroxide; thionyl chloride; sodium acetate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether;
DOI:10.1248/cpb.37.1852

Reference yield:

: 61289-17-6
methyl 3α-acetoxy-5β-chol-6-en-24-oate

: 114882-48-3
5β-cholestane-3α,6β,7α,25,26-pentol

Guidance literature:: Multi-step reaction with 14 steps

1: 5percent KOH in MeOH / 0.5 h

2: 4 h / 55 °C

3: SOCl₂ / 2 h / Ambient temperature

4: diethyl ether

5: collidine / 0.25 h / 180 - 200 °C

6: 10percent KOH in MeOH / 1 h / Heating

7: diethyl ether / 2 h

8: 1) m-chloroperbenzoic acid, 2) AcOH / 1) CHCl₃, 24 h, RT, 2) reflux, 3.5 h

9: 5percent KOH in MeOH / 1 h / Heating

10: NaOAc / 100 °C / Heating

11: SOCl₂

12: diethyl ether / Ambient temperature

13: 24 h / Ambient temperature

14: diethyl ether / 1) reflux, 2.5 h, 2) RT, overnight

With 2,3,5-trimethyl-pyridine; potassium hydroxide; thionyl chloride; sodium acetate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether;
DOI:10.1248/cpb.37.1852

Reference yield:

: 125380-49-6
3α-hydroxy-26,27-dinor-5β-cholest-6-en-25-oic acid

: 114882-48-3
5β-cholestane-3α,6β,7α,25,26-pentol

Guidance literature:: Multi-step reaction with 8 steps

1: diethyl ether / 2 h

2: 1) m-chloroperbenzoic acid, 2) AcOH / 1) CHCl₃, 24 h, RT, 2) reflux, 3.5 h

3: 5percent KOH in MeOH / 1 h / Heating

4: NaOAc / 100 °C / Heating

5: SOCl₂

6: diethyl ether / Ambient temperature

7: 24 h / Ambient temperature

8: diethyl ether / 1) reflux, 2.5 h, 2) RT, overnight

With potassium hydroxide; thionyl chloride; sodium acetate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether;
DOI:10.1248/cpb.37.1852