Phenol, 2-methoxy-, benzenesulfonate

Base Information

• Chemical Name: Phenol, 2-methoxy-, benzenesulfonate
• CAS No.: 3900-91-2
• Molecular Formula: C13H12O4S
• Molecular Weight: 264.302
• Hs Code.: 2909499000
• Mol file: 3900-91-2.mol

Synonyms:Guajacolbenzolsulfonat;Brenzcatechin-methylaether-benzolsulfonat;1-Benzolsulfonyloxy-2-methoxy-benzol;1-benzenesulfonyloxy-2-methoxy-benzene;Pyrocatechol methylether benzolsulphonat;

Chemical Property of Phenol, 2-methoxy-, benzenesulfonate

Chemical Property:

• PSA: 60.98000
• LogP: 3.54370

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenol, 2-methoxy-, benzenesulfonate

There total 3 articles about Phenol, 2-methoxy-, benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-methoxy-phenol (90-05-1) + benzenesulfonyl chloride (98-09-9) → 2-methoxyphenyl benzenesulfonate (3900-91-2)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 6h; Inert atmosphere;

DOI:10.1080/00397911.2017.1393088

Reference yield:

1,2-dimethoxybenzene (91-16-7) + benzenesulfonyl chloride (98-09-9) → 2-methoxyphenyl benzenesulfonate (3900-91-2) + 1,2-dimethoxy-4-(phenylsulfonyl)benzene (148808-80-4)

Guidance literature:

With zinc(II) chloride; at 110 ℃;

DOI:10.1039/jr9450000014

Reference yield:

→ 2-methoxyphenyl benzenesulfonate (3900-91-2)

Guidance literature:

Pyrocatechol mono benzolsulphonat, Dimethylsulphat;

DOI:10.1039/jr9650002651

upstream raw materials:

2-methoxy-phenol

benzenesulfonyl chloride

1,2-dimethoxybenzene

Downstream raw materials:

N-benzyl-2-methoxyaniline

1-(2-methoxyphenyl)-3,3-dimethyl-2-butanone

2-methoxy-benzonitrile

2-methoxy-phenol